methyl N-(tert-butoxycarbonyl)-3-methyl-L-phenylalanylglycinate

Base Information

Chemical Name:methyl N-(tert-butoxycarbonyl)-3-methyl-L-phenylalanylglycinate
CAS No.:1534361-82-4
Molecular Formula:C₁₈H₂₆N₂O₅
Molecular Weight:350.415
Hs Code.:

Synonyms:methyl N-(tert-butoxycarbonyl)-3-methyl-L-phenylalanylglycinate

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Chemical Property of methyl N-(tert-butoxycarbonyl)-3-methyl-L-phenylalanylglycinate

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Technology Process of methyl N-(tert-butoxycarbonyl)-3-methyl-L-phenylalanylglycinate

There total 1 articles about methyl N-(tert-butoxycarbonyl)-3-methyl-L-phenylalanylglycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 114873-06-2
(S)-2-((tert-butoxycarbonyl)amino)-3-(m-tolyl)propanoic acid

: 1534361-82-4
methyl N-(tert-butoxycarbonyl)-3-methyl-L-phenylalanylglycinate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1021/jm4016735

Reference yield: 100.0%

: 1534361-82-4
methyl N-(tert-butoxycarbonyl)-3-methyl-L-phenylalanylglycinate

: 1534361-83-5
3-(3-methylbenzyl)-2,5-piperazinedione

Guidance literature:: methyl N-(tert-butoxycarbonyl)-3-methyl-L-phenylalanylglycinate; In dichloromethane; trifluoroacetic acid;

With triethylamine; In methanol; at 70 ℃; Heating;
DOI:10.1021/jm4016735

Reference yield:

: 1534361-82-4
methyl N-(tert-butoxycarbonyl)-3-methyl-L-phenylalanylglycinate

: 3-(3-methylbenzyl)-1-(2-thiophenylsulfonyl)piperazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane; trifluoroacetic acid

1.2: 70 °C / Heating

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 70 °C / Heating

3.1: triethylamine / dichloromethane

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane; trifluoroacetic acid;
DOI:10.1021/jm4016735