C₁₄H₁₀FN₃

Base Information

Chemical Name:C₁₄H₁₀FN₃
CAS No.:1449278-76-5
Molecular Formula:C₁₄H₁₀FN₃
Molecular Weight:239.252
Hs Code.:

C<sub>14</sub>H<sub>10</sub>FN<sub>3</sub>

Synonyms:C₁₄H₁₀FN₃

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Chemical Property of C₁₄H₁₀FN₃

Chemical Property:

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Technology Process of C₁₄H₁₀FN₃

There total 7 articles about C₁₄H₁₀FN₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449278-74-3
C₂₄H₂₅FIN₃O₄

: 73183-34-3
bis(pinacol)diborane

: 1449278-75-4
C₃₀H₃₇BFN₃O₆

: 1449278-76-5
C₁₄H₁₀FN₃

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 90 ℃; for 2h; Inert atmosphere; Sealed tube;

Reference yield:

: 1449278-46-9
5-bromo-7-(2-trimethylsilylethoxymethyl)-1,7-naphthyridin-8-one

: 1449278-75-4
C₃₀H₃₇BFN₃O₆

: 1449278-76-5
C₁₄H₁₀FN₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: potassium carbonate; N,N-dimethyl-formamide; palladium diacetate; 1,3-bis(dicyclohexylphosphine)propane / 3 h / 85 °C

2.1: urea hydrogen peroxide adduct / dichloromethane / 0.08 h / 20 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

3.1: oxalyl dichloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

4.1: bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); potassium phosphate / 1,4-dioxane; water / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

6.1: trichlorophosphate / 3 h / 100 °C / Inert atmosphere

7.1: ammonia / isopropyl alcohol / 1.33 h / 140 °C / Inert atmosphere; Microwave irradiation

8.1: water; sodium hydroxide / methanol / 2 h / 50 °C / Inert atmosphere

9.1: N-iodo-succinimide; [bis(acetoxy)iodo]benzene / acetonitrile; water / 0.67 h / 60 °C / Inert atmosphere

10.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

11.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 2 h / 90 °C / Inert atmosphere; Sealed tube

With dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; N-iodo-succinimide; oxalyl dichloride; [bis(acetoxy)iodo]benzene; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); 1,3-bis(dicyclohexylphosphine)propane; tetrabutyl ammonium fluoride; ammonia; water; potassium acetate; palladium diacetate; urea hydrogen peroxide adduct; potassium carbonate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; isopropyl alcohol; acetonitrile;

Reference yield:

: 1449278-47-0
ethyl 8-oxo-7-(2-trimethylsilylethoxymethyl)-1,7-naphthyridine-5-carboxylate

: 1449278-75-4
C₃₀H₃₇BFN₃O₆

: 1449278-76-5
C₁₄H₁₀FN₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: urea hydrogen peroxide adduct / dichloromethane / 0.08 h / 20 °C / Inert atmosphere

1.2: 0.5 h / 20 °C / Inert atmosphere

2.1: oxalyl dichloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

3.1: bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); potassium phosphate / 1,4-dioxane; water / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

5.1: trichlorophosphate / 3 h / 100 °C / Inert atmosphere

6.1: ammonia / isopropyl alcohol / 1.33 h / 140 °C / Inert atmosphere; Microwave irradiation

7.1: water; sodium hydroxide / methanol / 2 h / 50 °C / Inert atmosphere

8.1: N-iodo-succinimide; [bis(acetoxy)iodo]benzene / acetonitrile; water / 0.67 h / 60 °C / Inert atmosphere

9.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

10.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 2 h / 90 °C / Inert atmosphere; Sealed tube

With dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; N-iodo-succinimide; oxalyl dichloride; [bis(acetoxy)iodo]benzene; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); tetrabutyl ammonium fluoride; ammonia; water; potassium acetate; urea hydrogen peroxide adduct; N-ethyl-N,N-diisopropylamine; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; isopropyl alcohol; acetonitrile;