(E)-3-((2-methylthiazol-4-yl)ethynyl)cyclohex-2-enone o-2-(2-(tert-butyldimethylsilyloxy)ethoxy)ethyl oxime

Base Information

• Chemical Name: (E)-3-((2-methylthiazol-4-yl)ethynyl)cyclohex-2-enone o-2-(2-(tert-butyldimethylsilyloxy)ethoxy)ethyl oxime
• CAS No.: 1239586-84-5
• Molecular Formula: C₂₂H₃₄N₂O₃SSi
• Molecular Weight: 434.675
• Mol file: 1239586-84-5.mol

Synonyms:(E)-3-((2-methylthiazol-4-yl)ethynyl)cyclohex-2-enone o-2-(2-(tert-butyldimethylsilyloxy)ethoxy)ethyl oxime

Chemical Property of (E)-3-((2-methylthiazol-4-yl)ethynyl)cyclohex-2-enone o-2-(2-(tert-butyldimethylsilyloxy)ethoxy)ethyl oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-3-((2-methylthiazol-4-yl)ethynyl)cyclohex-2-enone o-2-(2-(tert-butyldimethylsilyloxy)ethoxy)ethyl oxime

There total 1 articles about (E)-3-((2-methylthiazol-4-yl)ethynyl)cyclohex-2-enone o-2-(2-(tert-butyldimethylsilyloxy)ethoxy)ethyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

(2-(2-bromoethoxy)ethoxy)(tert-butyl)dimethylsilane + (E)-3-((2-methylthiazol-4-yl)ethynyl)cyclohex-2-enone oxime (1239586-80-1) → (E)-3-((2-methylthiazol-4-yl)ethynyl)cyclohex-2-enone o-2-(2-(tert-butyldimethylsilyloxy)ethoxy)ethyl oxime (1239586-84-5)

Guidance literature:

(E)-3-((2-methylthiazol-4-yl)ethynyl)cyclohex-2-enone oxime; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃;

(2-(2-bromoethoxy)ethoxy)(tert-butyl)dimethylsilane; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 2h;

DOI:10.1016/j.bmc.2010.06.070

Reference yield:

(E)-3-((2-methylthiazol-4-yl)ethynyl)cyclohex-2-enone o-2-(2-(tert-butyldimethylsilyloxy)ethoxy)ethyl oxime (1239586-84-5) → C16H20N2O3S

Guidance literature:

With tetrabutyl ammonium fluoride; water; In tetrahydrofuran; at 20 ℃; for 1.5h;

DOI:10.1016/j.bmc.2010.06.070

upstream raw materials:

(E)-3-((2-methylthiazol-4-yl)ethynyl)cyclohex-2-enone oxime