2-(5-(indolin-1-ylsulfonyl)-2-methoxyphenyl)-2-isobutyl-4-methylpentanenitrile

Base Information

Chemical Name:2-(5-(indolin-1-ylsulfonyl)-2-methoxyphenyl)-2-isobutyl-4-methylpentanenitrile
CAS No.:1620581-29-4
Molecular Formula:C₂₅H₃₂N₂O₃S
Molecular Weight:440.607
Hs Code.:

Synonyms:2-(5-(indolin-1-ylsulfonyl)-2-methoxyphenyl)-2-isobutyl-4-methylpentanenitrile

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Chemical Property of 2-(5-(indolin-1-ylsulfonyl)-2-methoxyphenyl)-2-isobutyl-4-methylpentanenitrile

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Technology Process of 2-(5-(indolin-1-ylsulfonyl)-2-methoxyphenyl)-2-isobutyl-4-methylpentanenitrile

There total 3 articles about 2-(5-(indolin-1-ylsulfonyl)-2-methoxyphenyl)-2-isobutyl-4-methylpentanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 496-15-1
1-indoline

: 1620581-27-2
C₁₇H₂₄ClNO₃S

: 1620581-29-4
2-(5-(indolin-1-ylsulfonyl)-2-methoxyphenyl)-2-isobutyl-4-methylpentanenitrile

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 23 ℃;
DOI:10.1021/ja505737x

Reference yield:

: 1620581-25-0
C₁₇H₂₅NO

: 1620581-29-4
2-(5-(indolin-1-ylsulfonyl)-2-methoxyphenyl)-2-isobutyl-4-methylpentanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / chloroform / 1.5 h / 0 - 23 °C

2: triethylamine / dichloromethane / 0 - 23 °C

With chlorosulfonic acid; triethylamine; In dichloromethane; chloroform;
DOI:10.1021/ja505737x

Reference yield:

: 7035-03-2
2-methoxy-benzeneacetonitrile

: 1620581-29-4
2-(5-(indolin-1-ylsulfonyl)-2-methoxyphenyl)-2-isobutyl-4-methylpentanenitrile

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 23 °C

2: chlorosulfonic acid / chloroform / 1.5 h / 0 - 23 °C

3: triethylamine / dichloromethane / 0 - 23 °C

With chlorosulfonic acid; sodium hydride; triethylamine; In dichloromethane; chloroform; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja505737x