2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophen-5-al

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Chemical Name:2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophen-5-al
CAS No.:1342894-98-7
Molecular Formula:C₂₇H₁₉Br₂NO₃S
Molecular Weight:597.327
Hs Code.:

Synonyms:2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophen-5-al

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Chemical Property of 2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophen-5-al

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Technology Process of 2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophen-5-al

There total 3 articles about 2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophen-5-al which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.3%

: 1342894-97-6
2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1342894-98-7
2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophen-5-al

Guidance literature:: With trichlorophosphate; In 1,2-dichloro-ethane; at 0 ℃; for 12h; Inert atmosphere; Reflux;
DOI:10.1016/j.polymer.2011.09.022

Reference yield:

: 1342894-95-4
diethyl ((4-(diphenylamino)benzyl)triphenyl)phosphonate

: 1342894-98-7
2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophen-5-al

Guidance literature:: Multi-step reaction with 2 steps

2: trichlorophosphate / 1,2-dichloro-ethane / 0 - 45 °C

With trichlorophosphate; In 1,2-dichloro-ethane; 1: Wittig reaction / 2: Vilsmeier formylation;
DOI:10.1002/chem.201102376

Reference yield:

: 204905-77-1
3,4-ethylenedioxythiophene-2-carboxaldehyde

: 1342894-98-7
2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophen-5-al

Guidance literature:: Multi-step reaction with 2 steps

2: trichlorophosphate / 1,2-dichloro-ethane / 0 - 45 °C

With trichlorophosphate; In 1,2-dichloro-ethane; 1: Wittig reaction / 2: Vilsmeier formylation;
DOI:10.1002/chem.201102376