2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophene

Base Information

Chemical Name:2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophene
CAS No.:1342894-97-6
Molecular Formula:C₂₆H₁₉Br₂NO₂S
Molecular Weight:569.316
Hs Code.:

Synonyms:2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophene

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Chemical Property of 2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophene

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Technology Process of 2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophene

There total 1 articles about 2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1342894-95-4
diethyl ((4-(diphenylamino)benzyl)triphenyl)phosphonate

: 204905-77-1
3,4-ethylenedioxythiophene-2-carboxaldehyde

: 1342894-97-6
2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophene

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.polymer.2011.09.022

Reference yield: 87.3%

: 1342894-97-6
2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1342894-98-7
2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophen-5-al

Guidance literature:: With trichlorophosphate; In 1,2-dichloro-ethane; at 0 ℃; for 12h; Inert atmosphere; Reflux;
DOI:10.1016/j.polymer.2011.09.022

Reference yield:

: 1342894-97-6
2-[2-[4-[N,N-di(4-bromophenyl)amino]phenyl]ethenyl]3,4-ethylenedioxythiophene

: C₂₇H₂₀Br₂NO₆S₂^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 1,2-dichloro-ethane / 0 - 45 °C

2: sodium hydrogensulfite / tetrahydrofuran / 20 °C / pH 5

With sodium hydrogensulfite; trichlorophosphate; In tetrahydrofuran; 1,2-dichloro-ethane; 1: |Vilsmeier Reaction;
DOI:10.1002/bio.3117