6-(4'-ethynylbenzoyl)-2,2,4,4-tetramethylperhydroazirino[1,2-c]imidazole-3-oxyl

Base Information

Chemical Name:6-(4'-ethynylbenzoyl)-2,2,4,4-tetramethylperhydroazirino[1,2-c]imidazole-3-oxyl
CAS No.:278183-99-6
Molecular Formula:C₁₇H₁₉N₂O₂
Molecular Weight:283.35
Hs Code.:

Synonyms:6-(4'-ethynylbenzoyl)-2,2,4,4-tetramethylperhydroazirino[1,2-c]imidazole-3-oxyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(4'-ethynylbenzoyl)-2,2,4,4-tetramethylperhydroazirino[1,2-c]imidazole-3-oxyl

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Technology Process of 6-(4'-ethynylbenzoyl)-2,2,4,4-tetramethylperhydroazirino[1,2-c]imidazole-3-oxyl

There total 4 articles about 6-(4'-ethynylbenzoyl)-2,2,4,4-tetramethylperhydroazirino[1,2-c]imidazole-3-oxyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 278184-08-0
C₁₇H₁₉N₂O₂

: 278183-99-6
6-(4'-ethynylbenzoyl)-2,2,4,4-tetramethylperhydroazirino[1,2-c]imidazole-3-oxyl

: 278184-13-7
4-(4'-ethynylphenacetylidene)-2,2,5,5-tetramethylimidazolidine-1-oxyl

Guidance literature:: With sodium hydroxide; In methanol; at 70 ℃; for 6h;
DOI:10.1007/bf02499075

Reference yield:

: 935-14-8
1,4-diethynylbenzene

: 278183-99-6
6-(4'-ethynylbenzoyl)-2,2,4,4-tetramethylperhydroazirino[1,2-c]imidazole-3-oxyl

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / CHCl₃ / 2 h / 50 °C

2: 15 percent / 15 percent NaOH / methanol / 6 h / 70 °C

With sodium hydroxide; In methanol; chloroform; 1: Cycloaddition / 2: Ring cleavage;
DOI:10.1007/bf02499075

Reference yield:

: 33452-43-6
2,2,5,5-tetramethyl-2,5-dihydro-1H-imidazol-1-oxyl 3-oxide

: 278183-99-6
6-(4'-ethynylbenzoyl)-2,2,4,4-tetramethylperhydroazirino[1,2-c]imidazole-3-oxyl

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / CHCl₃ / 2 h / 50 °C

2: 15 percent / 15 percent NaOH / methanol / 6 h / 70 °C

With sodium hydroxide; In methanol; chloroform; 1: Cycloaddition / 2: Ring cleavage;
DOI:10.1007/bf02499075