Technology Process of trans-1-phenyl-4-(p-nitrophenyl)-4-diazobut-1-ene
There total 6 articles about trans-1-phenyl-4-(p-nitrophenyl)-4-diazobut-1-ene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) potassium tert-butoxide / 1.) xylene, 25 deg C, 1 h, 2.) reflux, 24 h
2: 30 percent / N-chlorosuccinimide, silver nitrate / acetonitrile; H2O / 0.08 h / 25 °C
3: 190 mg / tetrahydrofuran / 96 h / Ambient temperature
4: 1.) sodium hydride / 1.) THF, 25 deg C, 20 min, 2.) benzene, reflux, 20 min
With
N-chloro-succinimide; potassium tert-butylate; sodium hydride; silver nitrate;
In
tetrahydrofuran; water; acetonitrile;
DOI:10.1021/ja00342a049
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 190 mg / tetrahydrofuran / 96 h / Ambient temperature
2: 1.) sodium hydride / 1.) THF, 25 deg C, 20 min, 2.) benzene, reflux, 20 min
With
sodium hydride;
In
tetrahydrofuran;
DOI:10.1021/ja00342a049
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 65 percent / hydrogen chloride gas / CHCl3 / 12 h / Ambient temperature
2: 1.) potassium tert-butoxide / 1.) xylene, 25 deg C, 1 h, 2.) reflux, 24 h
3: 30 percent / N-chlorosuccinimide, silver nitrate / acetonitrile; H2O / 0.08 h / 25 °C
4: 190 mg / tetrahydrofuran / 96 h / Ambient temperature
5: 1.) sodium hydride / 1.) THF, 25 deg C, 20 min, 2.) benzene, reflux, 20 min
With
hydrogenchloride; N-chloro-succinimide; potassium tert-butylate; sodium hydride; silver nitrate;
In
tetrahydrofuran; chloroform; water; acetonitrile;
DOI:10.1021/ja00342a049
