C₂₁H₁₈N₂O₅

Base Information

Chemical Name:C₂₁H₁₈N₂O₅
CAS No.:1380111-83-0
Molecular Formula:C₂₁H₁₈N₂O₅
Molecular Weight:378.384
Hs Code.:

C<sub>21</sub>H<sub>18</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₁H₁₈N₂O₅

Suppliers and Price of C₂₁H₁₈N₂O₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₁H₁₈N₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₁H₁₈N₂O₅

There total 7 articles about C₂₁H₁₈N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1380111-82-9
C₂₉H₂₆N₂O₆

: 1380111-83-0
C₂₁H₁₈N₂O₅

Guidance literature:: C₂₉H₂₆N₂O₆; With water; lithium hydroxide; In tetrahydrofuran; at 20 - 25 ℃; for 20h;

With hydrogenchloride; In tetrahydrofuran; water; at 20 - 25 ℃; for 31h;

Reference yield:

: 501-30-4,123712-78-7
5-hydroxy-2-(hydroxymethyl)-4H-pyran-4-one

: 1380111-83-0
C₂₁H₁₈N₂O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydroxide / methanol; water / Reflux

2.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C

3.1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 - 25 °C

4.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 3 h / 0 °C

5.1: sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene / water; acetonitrile / 0.75 h / 0 °C

6.1: 1,1'-carbonyldiimidazole / N,N-dimethyl acetamide / 4 h / 20 - 25 °C

6.2: 17 h / 20 - 25 °C

7.1: water; lithium hydroxide / tetrahydrofuran / 20 h / 20 - 25 °C

7.2: 31 h / 20 - 25 °C

With sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene; hydroxylamine hydrochloride; water; sodium acetate; sulfur trioxide pyridine complex; potassium carbonate; dimethyl sulfoxide; triethylamine; 1,1'-carbonyldiimidazole; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl acetamide; water; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 1380109-74-9
C₂₀H₁₉NO₄

: 1380111-83-0
C₂₁H₁₈N₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 3 h / 0 °C

2.1: sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene / water; acetonitrile / 0.75 h / 0 °C

3.1: 1,1'-carbonyldiimidazole / N,N-dimethyl acetamide / 4 h / 20 - 25 °C

3.2: 17 h / 20 - 25 °C

4.1: water; lithium hydroxide / tetrahydrofuran / 20 h / 20 - 25 °C

4.2: 31 h / 20 - 25 °C

With sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene; water; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; 1,1'-carbonyldiimidazole; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water; acetonitrile;