(3R,3aR)-phenyl 7-bromo-4-oxo-3a,4-dihydro-3H-benzo[b]imidazo[1,5-d][1,4]oxazine-3-carboxylate

Base Information

Chemical Name:(3R,3aR)-phenyl 7-bromo-4-oxo-3a,4-dihydro-3H-benzo[b]imidazo[1,5-d][1,4]oxazine-3-carboxylate
CAS No.:1630973-35-1
Molecular Formula:C₁₇H₁₁BrN₂O₄
Molecular Weight:387.189
Hs Code.:

Synonyms:(3R,3aR)-phenyl 7-bromo-4-oxo-3a,4-dihydro-3H-benzo[b]imidazo[1,5-d][1,4]oxazine-3-carboxylate

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Chemical Property of (3R,3aR)-phenyl 7-bromo-4-oxo-3a,4-dihydro-3H-benzo[b]imidazo[1,5-d][1,4]oxazine-3-carboxylate

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Technology Process of (3R,3aR)-phenyl 7-bromo-4-oxo-3a,4-dihydro-3H-benzo[b]imidazo[1,5-d][1,4]oxazine-3-carboxylate

There total 2 articles about (3R,3aR)-phenyl 7-bromo-4-oxo-3a,4-dihydro-3H-benzo[b]imidazo[1,5-d][1,4]oxazine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1630972-75-6
7-bromo-2H-benzo[b][1,4]oxazin-2-one

: 1630972-39-2
phenyl isocyanoacetate

: 1630973-35-1
(3R,3aR)-phenyl 7-bromo-4-oxo-3a,4-dihydro-3H-benzo[b]imidazo[1,5-d][1,4]oxazine-3-carboxylate

Guidance literature:: With C₃₉H₃₈N₃O₂P; silver(l) oxide; In tetrahydrofuran; at -20 ℃; for 24h; stereoselective reaction;
DOI:10.1002/anie.201402788

Reference yield:

: 38191-34-3
2-amino-5-bromophenol

: 1630973-35-1
(3R,3aR)-phenyl 7-bromo-4-oxo-3a,4-dihydro-3H-benzo[b]imidazo[1,5-d][1,4]oxazine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 24 h / Molecular sieve; Reflux

2: C₃₉H₃₈N₃O₂P; silver(l) oxide / tetrahydrofuran / 24 h / -20 °C

With C₃₉H₃₈N₃O₂P; silver(l) oxide; In tetrahydrofuran; toluene;
DOI:10.1002/anie.201402788