N-[3,5-bis((3,5-bis(benzyloxy))benzyloxy)benzaylidene]-N'-tosylhydrazone

Base Information

Chemical Name:N-[3,5-bis((3,5-bis(benzyloxy))benzyloxy)benzaylidene]-N'-tosylhydrazone
CAS No.:804477-13-2
Molecular Formula:C₅₆H₅₀N₂O₈S
Molecular Weight:911.088
Hs Code.:

Synonyms:N-[3,5-bis((3,5-bis(benzyloxy))benzyloxy)benzaylidene]-N'-tosylhydrazone

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Chemical Property of N-[3,5-bis((3,5-bis(benzyloxy))benzyloxy)benzaylidene]-N'-tosylhydrazone

Chemical Property:

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Technology Process of N-[3,5-bis((3,5-bis(benzyloxy))benzyloxy)benzaylidene]-N'-tosylhydrazone

There total 6 articles about N-[3,5-bis((3,5-bis(benzyloxy))benzyloxy)benzaylidene]-N'-tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 137472-18-5
3,5-bis(3,5-bis(benzyloxy)benzyloxy)benzaldehyde

: 804477-13-2
N-[3,5-bis((3,5-bis(benzyloxy))benzyloxy)benzaylidene]-N'-tosylhydrazone

Guidance literature:: In diethyl ether; ethanol; for 12h; Heating;
DOI:10.1021/ja046965q

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 804477-13-2
N-[3,5-bis((3,5-bis(benzyloxy))benzyloxy)benzaylidene]-N'-tosylhydrazone

Guidance literature:: Multi-step reaction with 6 steps

1: K₂CO₃ / acetone / 16 h / Heating

2: LiAlH₄ / tetrahydrofuran / 30 °C

3: PBr₃; pyridine / CH₂Cl₂

4: K₂CO₃ / acetone / 16 h / Heating

5: pyridinium chlorochromate / CH₂Cl₂ / 1 h

6: 86 percent / ethanol; diethyl ether / 12 h / Heating

With pyridine; lithium aluminium tetrahydride; phosphorus tribromide; potassium carbonate; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; acetone;
DOI:10.1021/ja046965q

Reference yield:

: 24131-32-6
3,5-bis(benzyloxy)benzyl bromide

: 804477-13-2
N-[3,5-bis((3,5-bis(benzyloxy))benzyloxy)benzaylidene]-N'-tosylhydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / acetone / 16 h / Heating

2: pyridinium chlorochromate / CH₂Cl₂ / 1 h

3: 86 percent / ethanol; diethyl ether / 12 h / Heating

With potassium carbonate; pyridinium chlorochromate; In diethyl ether; ethanol; dichloromethane; acetone;
DOI:10.1021/ja046965q