Technology Process of C18H31NO3
There total 6 articles about C18H31NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrazine hydrate;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 12h;
DOI:10.1021/jacs.9b06739
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / acetonitrile / 0.5 h / 20 °C / Inert atmosphere
1.2: Inert atmosphere; Reflux
2.1: sodium azide / acetone; water / 24 h / Inert atmosphere; Reflux
3.1: palladium on activated charcoal; hydrogen / methanol; chloroform / 24 h / Reflux
With
sodium azide; palladium on activated charcoal; hydrogen; potassium carbonate;
In
methanol; chloroform; water; acetone; acetonitrile;
DOI:10.1039/c3cc48014c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide / acetone; water / 24 h / Inert atmosphere; Reflux
2: palladium on activated charcoal; hydrogen / methanol; chloroform / 24 h / Reflux
With
sodium azide; palladium on activated charcoal; hydrogen;
In
methanol; chloroform; water; acetone;
DOI:10.1039/c3cc48014c