3,5-dimethyl-N-(phenyl-thiocarbamoyl)-pyrazole-1-carboximidic acid amide

Base Information

• Chemical Name: 3,5-dimethyl-N-(phenyl-thiocarbamoyl)-pyrazole-1-carboximidic acid amide
• CAS No.: 108754-33-2
• Molecular Formula: C₁₃H₁₅N₅S
• Molecular Weight: 273.362

Synonyms:3,5-dimethyl-N-(phenyl-thiocarbamoyl)-pyrazole-1-carboximidic acid amide

Chemical Property of 3,5-dimethyl-N-(phenyl-thiocarbamoyl)-pyrazole-1-carboximidic acid amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-dimethyl-N-(phenyl-thiocarbamoyl)-pyrazole-1-carboximidic acid amide

There total 4 articles about 3,5-dimethyl-N-(phenyl-thiocarbamoyl)-pyrazole-1-carboximidic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

3,5-dimethyl-1-pyrazolylformaminidium nitrate (38184-47-3) + phenyl isothiocyanate (103-72-0) → 3,5-dimethyl-N-(phenyl-thiocarbamoyl)-pyrazole-1-carboximidic acid amide (108754-33-2)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; at 50 - 60 ℃; for 1h;

DOI:10.1080/00397919708005647

Reference yield:

acetylacetone (123-54-6,81235-32-7) → 3,5-dimethyl-N-(phenyl-thiocarbamoyl)-pyrazole-1-carboximidic acid amide (108754-33-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous ethanol; aqueous KOH

2: ethanol

With potassium hydroxide; ethanol;

DOI:10.1021/ja01138a032

Reference yield:

3,5-Dimethylpyrazole-1-carboxamidine (22906-75-8) + phenyl isothiocyanate (103-72-0) → 3,5-dimethyl-N-(phenyl-thiocarbamoyl)-pyrazole-1-carboximidic acid amide (108754-33-2)

Guidance literature:

With ethanol;

DOI:10.1021/ja01138a032

upstream raw materials:

3,5-Dimethylpyrazole-1-carboxamidine

phenyl isothiocyanate

3,5-dimethyl-1-pyrazolylformaminidium nitrate

acetylacetone

Downstream raw materials:

[3-(3,5-dimethyl-pyrazol-1-yl)-[1,2,4]thiadiazol-5-yl]-phenyl-amine

(4-amino-2-phenylaminothiazol-5-yl)phenylmethanone

N³-phenyl-1H-[1,2,4]triazole-3,5-diamine

1-Diaminomethylene-3-phenyl-thiourea

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 108754-33-2 3,5-dimethyl-N-(phenyl-thiocarbamoyl)-pyrazole-1-carboximidic acid amide

Send

Send

Metric Ton KG G Pound L ML

Send

Send