N-(6-(dimethylamino)-9-(4-nitrophenyl)-3H-xanthen-3-ylidene)-N-methylmethanaminium trifluoroacetate

Base Information

Chemical Name:N-(6-(dimethylamino)-9-(4-nitrophenyl)-3H-xanthen-3-ylidene)-N-methylmethanaminium trifluoroacetate
CAS No.:1427006-10-7
Molecular Formula:C₂F₃O₂*C₂₃H₂₂N₃O₃
Molecular Weight:501.462
Hs Code.:

Synonyms:N-(6-(dimethylamino)-9-(4-nitrophenyl)-3H-xanthen-3-ylidene)-N-methylmethanaminium trifluoroacetate

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Chemical Property of N-(6-(dimethylamino)-9-(4-nitrophenyl)-3H-xanthen-3-ylidene)-N-methylmethanaminium trifluoroacetate

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Technology Process of N-(6-(dimethylamino)-9-(4-nitrophenyl)-3H-xanthen-3-ylidene)-N-methylmethanaminium trifluoroacetate

There total 3 articles about N-(6-(dimethylamino)-9-(4-nitrophenyl)-3H-xanthen-3-ylidene)-N-methylmethanaminium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 54764-79-3
6,6’-((4-nitrophenyl)methylene)bis(3-(dimethylamino)phenol)

: 76-05-1
trifluoroacetic acid

: 1427006-10-7
N-(6-(dimethylamino)-9-(4-nitrophenyl)-3H-xanthen-3-ylidene)-N-methylmethanaminium trifluoroacetate

Guidance literature:: 6,6’-((4-nitrophenyl)methylene)bis(3-(dimethylamino)phenol); With acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; at 20 ℃; for 3h; Inert atmosphere;

trifluoroacetic acid; In methanol; dichloromethane; Inert atmosphere;
DOI:10.1039/c3cc40616d

Reference yield:

: 99-07-0
3-Dimethylaminophenol

: 1427006-10-7
N-(6-(dimethylamino)-9-(4-nitrophenyl)-3H-xanthen-3-ylidene)-N-methylmethanaminium trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; toluene-4-sulfonic acid / 14 h / 60 °C / Inert atmosphere

2.1: acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 3 h / 20 °C / Inert atmosphere

2.2: Inert atmosphere

With toluene-4-sulfonic acid; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene;
DOI:10.1039/c3cc40616d

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 1427006-10-7
N-(6-(dimethylamino)-9-(4-nitrophenyl)-3H-xanthen-3-ylidene)-N-methylmethanaminium trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; toluene-4-sulfonic acid / 14 h / 60 °C / Inert atmosphere

2.1: acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 3 h / 20 °C / Inert atmosphere

2.2: Inert atmosphere

With toluene-4-sulfonic acid; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene;
DOI:10.1039/c3cc40616d