2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-3,5-dimethylphenol

Base Information

Chemical Name:2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-3,5-dimethylphenol
CAS No.:300766-99-8
Molecular Formula:C₁₇H₂₈O₂Si
Molecular Weight:292.494
Hs Code.:

Synonyms:2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-3,5-dimethylphenol

Suppliers and Price of 2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-3,5-dimethylphenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-3,5-dimethylphenol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-3,5-dimethylphenol

There total 4 articles about 2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-3,5-dimethylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 300766-98-7
2-[(Z)-3-hydroxy-1-propenyl]-3,5-dimethylphenol

: 300766-99-8
2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-3,5-dimethylphenol

Guidance literature:: With dmap; In tetrahydrofuran; at 0 ℃; for 8h;
DOI:10.1248/cpb.48.1138

Reference yield:

: 14002-99-4
5,7-dimethyl-2H-1-benzopyran-2-one

: 300766-99-8
2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-3,5-dimethylphenol

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / LAH / diethyl ether / 0.25 h / 0 °C

2: 91 percent / DMAP / tetrahydrofuran / 8 h / 0 °C

With dmap; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;
DOI:10.1248/cpb.48.1138

Reference yield:

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: 300766-99-8
2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-3,5-dimethylphenol

Guidance literature:: Multi-step reaction with 3 steps

1: CH₃SO₃H / 80 - 90 °C

2: lithium aluminum hydride / 15 h / 0 °C

3: 4-dimethylaminopyridine / tetrahydrofuran / 0 °C

With dmap; lithium aluminium tetrahydride; methanesulfonic acid; In tetrahydrofuran;
DOI:10.1016/S0960-894X(99)00289-9