{2-[(Z)-5-(tert-Butyl-diphenyl-silanyloxy)-hept-3-ene-1,6-diynyl]-phenyl}-methanol

Base Information

Chemical Name:{2-[(Z)-5-(tert-Butyl-diphenyl-silanyloxy)-hept-3-ene-1,6-diynyl]-phenyl}-methanol
CAS No.:207789-65-9
Molecular Formula:C₃₀H₃₀O₂Si
Molecular Weight:450.653
Hs Code.:

Synonyms:{2-[(Z)-5-(tert-Butyl-diphenyl-silanyloxy)-hept-3-ene-1,6-diynyl]-phenyl}-methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {2-[(Z)-5-(tert-Butyl-diphenyl-silanyloxy)-hept-3-ene-1,6-diynyl]-phenyl}-methanol

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Technology Process of {2-[(Z)-5-(tert-Butyl-diphenyl-silanyloxy)-hept-3-ene-1,6-diynyl]-phenyl}-methanol

There total 7 articles about {2-[(Z)-5-(tert-Butyl-diphenyl-silanyloxy)-hept-3-ene-1,6-diynyl]-phenyl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 207789-64-8
{2-[(Z)-5-(tert-Butyl-diphenyl-silanyloxy)-7-trimethylsilanyl-hept-3-ene-1,6-diynyl]-phenyl}-methanol

: 207789-65-9
{2-[(Z)-5-(tert-Butyl-diphenyl-silanyloxy)-hept-3-ene-1,6-diynyl]-phenyl}-methanol

Guidance literature:: With potassium carbonate; In methanol; for 4h; Ambient temperature;
DOI:10.1055/s-1998-1693

Reference yield:

: 10602-08-1
2-ethynylbenzyl alcohol

: 207789-65-9
{2-[(Z)-5-(tert-Butyl-diphenyl-silanyloxy)-hept-3-ene-1,6-diynyl]-phenyl}-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / i-Pr₂NH / Pd(PPh₃)2Cl₂, CuI / tetrahydrofuran / 2 h / Ambient temperature

2: 95 percent / K₂CO₃ / methanol / 4 h / Ambient temperature

With potassium carbonate; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; methanol;
DOI:10.1055/s-1998-1693

Reference yield:

: 77123-58-1
2-[2-(trimethylsilyl)ethynyl]benzaldehyde

: 207789-65-9
{2-[(Z)-5-(tert-Butyl-diphenyl-silanyloxy)-hept-3-ene-1,6-diynyl]-phenyl}-methanol

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄ / ethanol / 0.33 h / 0 °C

2: H₂O, NH₄F, n-Bu₄NHSO₄ / CH₂Cl₂ / 1 h / Ambient temperature

3: 95 percent / i-Pr₂NH / Pd(PPh₃)2Cl₂, CuI / tetrahydrofuran / 2 h / Ambient temperature

4: 95 percent / K₂CO₃ / methanol / 4 h / Ambient temperature

With ammonium fluoride; sodium tetrahydroborate; water; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1055/s-1998-1693