(2S,3R)-N-(2,4-dimethoxybenzyl)-N--2,3-epoxybutyramide

Base Information

Chemical Name:(2S,3R)-N-(2,4-dimethoxybenzyl)-N--2,3-epoxybutyramide
CAS No.:85725-64-0
Molecular Formula:C₂₀H₂₇NO₈
Molecular Weight:409.436
Hs Code.:

(2S,3R)-N-(2,4-dimethoxybenzyl)-N-<bis(ethoxycarbonyl)methyl>-2,3-epoxybutyramide

Synonyms:(2S,3R)-N-(2,4-dimethoxybenzyl)-N--2,3-epoxybutyramide

Suppliers and Price of (2S,3R)-N-(2,4-dimethoxybenzyl)-N--2,3-epoxybutyramide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,3R)-N-(2,4-dimethoxybenzyl)-N--2,3-epoxybutyramide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,3R)-N-(2,4-dimethoxybenzyl)-N--2,3-epoxybutyramide

There total 3 articles about (2S,3R)-N-(2,4-dimethoxybenzyl)-N--2,3-epoxybutyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 85725-58-2
(2R,3R)-N-(2,4-dimethoxybenzyl)-N--2-bromo-3-hydroxybutyramide

: 85725-64-0
(2S,3R)-N-(2,4-dimethoxybenzyl)-N--2,3-epoxybutyramide

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1246/cl.1983.169 DOI:10.1246/bcsj.57.2135

Reference yield:

: 81902-49-0
diethyl N-(2,4-dimethoxybenzyl)-amino-malonate

: 85725-64-0
(2S,3R)-N-(2,4-dimethoxybenzyl)-N--2,3-epoxybutyramide

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / tetrahydrofuran

2: EtOH-H₂O-HCl (9:2:1)

3: 86 percent / NaH / tetrahydrofuran / 0.5 h / 0 °C

With hydrogenchloride; sodium hydride; triethylamine; In tetrahydrofuran;
DOI:10.1246/cl.1983.169

Reference yield:

: 85725-69-5
(2R,3R)-N-(2,4-dimethoxybenzyl)-N--2-bromo-3-(t-butyldimethylsilyloxy)butyramide

: 85725-64-0
(2S,3R)-N-(2,4-dimethoxybenzyl)-N--2,3-epoxybutyramide

Guidance literature:: Multi-step reaction with 2 steps

1: EtOH-H₂O-HCl (9:2:1)

2: 86 percent / NaH / tetrahydrofuran / 0.5 h / 0 °C

With hydrogenchloride; sodium hydride; In tetrahydrofuran;
DOI:10.1246/cl.1983.169