(2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-2-azido-3-benzyloxyoctadec-4-ene

Base Information

Chemical Name:(2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-2-azido-3-benzyloxyoctadec-4-ene
CAS No.:1597422-26-8
Molecular Formula:C₇₄H₈₃N₃O₁₈
Molecular Weight:1302.48
Hs Code.:

Synonyms:(2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-2-azido-3-benzyloxyoctadec-4-ene

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Chemical Property of (2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-2-azido-3-benzyloxyoctadec-4-ene

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Technology Process of (2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-2-azido-3-benzyloxyoctadec-4-ene

There total 1 articles about (2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-2-azido-3-benzyloxyoctadec-4-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1445-45-0
Trimethyl orthoacetate

: 1597422-25-7
(2S,3R,4E)-2-azido-1-(4-O-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-3-benzyloxyoctadec-4-ene

: 1597422-26-8
(2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-2-azido-3-benzyloxyoctadec-4-ene

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1039/c4ob00241e

Reference yield: 56.0%

: 1597422-26-8
(2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-2-azido-3-benzyloxyoctadec-4-ene

: 150969-30-5
2,3-di-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl trichloroacetimidate

: (2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-3-O-(2,3-di-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-2-azido-3-benzyloxyoctadec-4-ene

Guidance literature:: (2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-2-azido-3-benzyloxyoctadec-4-ene; 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl trichloroacetimidate; In dichloromethane; for 0.5h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 2.5h; Molecular sieve; Inert atmosphere;
DOI:10.1039/c4ob00241e