2-[3-benzoyl-6-(toluene-4-sulfonylimino)-6H-pyridazin-1-yl]-2-phenylacetamide

Base Information

Chemical Name:2-[3-benzoyl-6-(toluene-4-sulfonylimino)-6H-pyridazin-1-yl]-2-phenylacetamide
CAS No.:591734-20-2
Molecular Formula:C₂₆H₂₂N₄O₄S
Molecular Weight:486.551
Hs Code.:

Synonyms:2-[3-benzoyl-6-(toluene-4-sulfonylimino)-6H-pyridazin-1-yl]-2-phenylacetamide

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Chemical Property of 2-[3-benzoyl-6-(toluene-4-sulfonylimino)-6H-pyridazin-1-yl]-2-phenylacetamide

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Technology Process of 2-[3-benzoyl-6-(toluene-4-sulfonylimino)-6H-pyridazin-1-yl]-2-phenylacetamide

There total 6 articles about 2-[3-benzoyl-6-(toluene-4-sulfonylimino)-6H-pyridazin-1-yl]-2-phenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-82-2
phenylacetic acid

: 591734-20-2
2-[3-benzoyl-6-(toluene-4-sulfonylimino)-6H-pyridazin-1-yl]-2-phenylacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / NBS; benzoyl peroxide / CCl₄ / 5 h / UV-irradiation; heating

2: oxalyl chloride; DMF / CH₂Cl₂ / 3 h

3: NH₃ gas / toluene; hexane / 1 h

4: 89 percent / DIPEA / dimethylformamide / 24 h

With N-Bromosuccinimide; oxalyl dichloride; ammonia; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; dibenzoyl peroxide; In tetrachloromethane; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm020583i

Reference yield:

: 4870-65-9,31302-84-8
2-bromophenylacetic acid

: 591734-20-2
2-[3-benzoyl-6-(toluene-4-sulfonylimino)-6H-pyridazin-1-yl]-2-phenylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride; DMF / CH₂Cl₂ / 3 h

2: NH₃ gas / toluene; hexane / 1 h

3: 89 percent / DIPEA / dimethylformamide / 24 h

With oxalyl dichloride; ammonia; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In hexane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm020583i

Reference yield:

: 19078-72-9
bromo(phenyl)acetyl chloride

: 591734-20-2
2-[3-benzoyl-6-(toluene-4-sulfonylimino)-6H-pyridazin-1-yl]-2-phenylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃ gas / toluene; hexane / 1 h

2: 89 percent / DIPEA / dimethylformamide / 24 h

With ammonia; N-ethyl-N,N-diisopropylamine; In hexane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm020583i