3,6-Bis-[1-phenyl-meth-(Z)-ylidene]-4-[1-phenyl-meth-(E)-ylidene]-cycloheptanone

Base Information

• Chemical Name: 3,6-Bis-[1-phenyl-meth-(Z)-ylidene]-4-[1-phenyl-meth-(E)-ylidene]-cycloheptanone
• CAS No.: 96095-46-4
• Molecular Formula: C₂₈H₂₄O
• Molecular Weight: 376.498

Synonyms:3,6-Bis-[1-phenyl-meth-(Z)-ylidene]-4-[1-phenyl-meth-(E)-ylidene]-cycloheptanone

Chemical Property of 3,6-Bis-[1-phenyl-meth-(Z)-ylidene]-4-[1-phenyl-meth-(E)-ylidene]-cycloheptanone

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Technology Process of 3,6-Bis-[1-phenyl-meth-(Z)-ylidene]-4-[1-phenyl-meth-(E)-ylidene]-cycloheptanone

There total 6 articles about 3,6-Bis-[1-phenyl-meth-(Z)-ylidene]-4-[1-phenyl-meth-(E)-ylidene]-cycloheptanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.5%

1-phenylpropadiene (2327-99-3) → 3-Methylene-2-phenyl-5-[1-phenyl-meth-(E)-ylidene]-cyclopentanone + C27H24 + 3-Methylene-2-phenyl-5-[1-phenyl-meth-(E)-ylidene]-6-[1-phenyl-meth-(Z)-ylidene]-cycloheptanone (96095-44-2) + 3,6-Bis-[1-phenyl-meth-(Z)-ylidene]-4-[1-phenyl-meth-(E)-ylidene]-cycloheptanone (96095-46-4)

Guidance literature:

With tris(triphenylphosphine)nickel⁽⁰⁾; carbon monoxide; In tetrahydrofuran; at 20 ℃; for 2.5h; Further byproducts given;

DOI:10.1021/ja00297a022

Reference yield: 8.5%

1-phenylpropadiene (2327-99-3) + carbon monoxide (201230-82-2) → (E)-4-benzylidene-3-methyl-2-phenylcyclopent-2-en-1-one (96095-49-7) + C27H24 + 3-Methylene-2-phenyl-5-[1-phenyl-meth-(E)-ylidene]-6-[1-phenyl-meth-(Z)-ylidene]-cycloheptanone (96095-44-2) + 3,6-Bis-[1-phenyl-meth-(Z)-ylidene]-4-[1-phenyl-meth-(E)-ylidene]-cycloheptanone (96095-46-4)

Guidance literature:

With tris(triphenylphosphine)nickel⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 2.5h; Further byproducts given;

DOI:10.1021/ja00297a022

Reference yield: 8.5%

1-phenylpropadiene (2327-99-3) + carbon monoxide (201230-82-2) → 3-Methylene-2-phenyl-5-[1-phenyl-meth-(E)-ylidene]-cyclopentanone + C27H24 + 3-Methylene-2-phenyl-5-[1-phenyl-meth-(E)-ylidene]-6-[1-phenyl-meth-(Z)-ylidene]-cycloheptanone (96095-44-2) + 3,6-Bis-[1-phenyl-meth-(Z)-ylidene]-4-[1-phenyl-meth-(E)-ylidene]-cycloheptanone (96095-46-4)

Guidance literature:

With tris(triphenylphosphine)nickel⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 2.5h; Further byproducts given;

DOI:10.1021/ja00297a022

upstream raw materials:

1-phenylpropadiene

carbon monoxide

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