4-Oxo-2-(2'-isobutyl-4'-methyl-phenyl)-1,2,3,4-tetrahydrophenanthren-1-carbonsaeure

Base Information

Chemical Name:4-Oxo-2-(2'-isobutyl-4'-methyl-phenyl)-1,2,3,4-tetrahydrophenanthren-1-carbonsaeure
CAS No.:68102-32-9
Molecular Formula:C₂₆H₂₆O₃
Molecular Weight:386.491
Hs Code.:

Synonyms:4-Oxo-2-(2'-isobutyl-4'-methyl-phenyl)-1,2,3,4-tetrahydrophenanthren-1-carbonsaeure

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Chemical Property of 4-Oxo-2-(2'-isobutyl-4'-methyl-phenyl)-1,2,3,4-tetrahydrophenanthren-1-carbonsaeure

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Technology Process of 4-Oxo-2-(2'-isobutyl-4'-methyl-phenyl)-1,2,3,4-tetrahydrophenanthren-1-carbonsaeure

There total 10 articles about 4-Oxo-2-(2'-isobutyl-4'-methyl-phenyl)-1,2,3,4-tetrahydrophenanthren-1-carbonsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5160-99-6
1-iso-butyl-3-methylbenzene

: 68102-32-9
4-Oxo-2-(2'-isobutyl-4'-methyl-phenyl)-1,2,3,4-tetrahydrophenanthren-1-carbonsaeure

Guidance literature:: Multi-step reaction with 7 steps

1: SnCl₄ / CS₂

2: H₂O, hexamethylenetetramine / ethanol

3: (i) Py, (ii) aq. Na₂CO₃, Et₂O

4: H₂SO₄

5: Na / ethanol

6: KOH / ethanol

7: SnCl₄

With potassium hydroxide; hexamethylenetetramine; sulfuric acid; water; sodium; tin(IV) chloride; In carbon disulfide; ethanol;

Reference yield:

: 625-95-6
3-Iodotoluene

: 68102-32-9
4-Oxo-2-(2'-isobutyl-4'-methyl-phenyl)-1,2,3,4-tetrahydrophenanthren-1-carbonsaeure

Guidance literature:: Multi-step reaction with 10 steps

1: (i) Mg, Et₂O, (ii) /BRN= 605330/

2: PBr₃

3: NaBH₄ / dimethylsulfoxide

4: SnCl₄ / CS₂

5: H₂O, hexamethylenetetramine / ethanol

6: (i) Py, (ii) aq. Na₂CO₃, Et₂O

7: H₂SO₄

8: Na / ethanol

9: KOH / ethanol

10: SnCl₄

With potassium hydroxide; sodium tetrahydroborate; hexamethylenetetramine; sulfuric acid; water; sodium; phosphorus tribromide; tin(IV) chloride; In carbon disulfide; ethanol; dimethyl sulfoxide;

Reference yield:

: 7315-74-4
2-methyl-1-(3-methylphenyl)propan-1-ol

: 68102-32-9
4-Oxo-2-(2'-isobutyl-4'-methyl-phenyl)-1,2,3,4-tetrahydrophenanthren-1-carbonsaeure

Guidance literature:: Multi-step reaction with 9 steps

1: PBr₃

2: NaBH₄ / dimethylsulfoxide

3: SnCl₄ / CS₂

4: H₂O, hexamethylenetetramine / ethanol

5: (i) Py, (ii) aq. Na₂CO₃, Et₂O

6: H₂SO₄

7: Na / ethanol

8: KOH / ethanol

9: SnCl₄

With potassium hydroxide; sodium tetrahydroborate; hexamethylenetetramine; sulfuric acid; water; sodium; phosphorus tribromide; tin(IV) chloride; In carbon disulfide; ethanol; dimethyl sulfoxide;