C₂₇H₃₆BrNO₈S

Base Information

Chemical Name:C₂₇H₃₆BrNO₈S
CAS No.:1571933-90-8
Molecular Formula:C₂₇H₃₆BrNO₈S
Molecular Weight:614.555
Hs Code.:

C<sub>27</sub>H<sub>36</sub>BrNO<sub>8</sub>S

Synonyms:C₂₇H₃₆BrNO₈S

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Chemical Property of C₂₇H₃₆BrNO₈S

Chemical Property:

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Technology Process of C₂₇H₃₆BrNO₈S

There total 10 articles about C₂₇H₃₆BrNO₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1571933-87-3
tert-butyl 2-(tert-butoxycarbonylamino)-3-(2-bromo-5-(2-(4-methylphenylsulfonyloxy)ethoxy)phenyl)propanoate

: 1571933-89-5
C₂₇H₃₆BrNO₈S

: 1571933-90-8
C₂₇H₃₆BrNO₈S

Guidance literature:: With Column: CHIRALPAC IA 20 mmφ×250 mm, manufactured by Daicel Corporation; In ethanol; hexane; at 25 ℃; Resolution of racemate;

Reference yield:

: 1571933-52-2
C₂₄H₄₀INO₅Si

: 1571933-89-5
C₂₇H₃₆BrNO₈S

: 1571933-90-8
C₂₇H₃₆BrNO₈S

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride / toluene / 6 h / 100 °C / Inert atmosphere

2: bromine / methanol; diethyl ether / 0.5 h / -70 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

4: potassium carbonate / acetone / 23 h / Reflux

5: Column: CHIRALPAC IA 20 mmφ×250 mm, manufactured by Daicel Corporation / hexane; ethanol / 25 °C / Resolution of racemate

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; bromine; potassium carbonate; lithium chloride; In tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; acetone; toluene;

Reference yield:

: 1571933-96-4
C₂₇H₄₉NO₅SiSn

: 1571933-89-5
C₂₇H₃₆BrNO₈S

: 1571933-90-8
C₂₇H₃₆BrNO₈S

Guidance literature:: Multi-step reaction with 4 steps

1: bromine / methanol; diethyl ether / 0.5 h / -70 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

3: potassium carbonate / acetone / 23 h / Reflux

4: Column: CHIRALPAC IA 20 mmφ×250 mm, manufactured by Daicel Corporation / hexane; ethanol / 25 °C / Resolution of racemate

With tetrabutyl ammonium fluoride; bromine; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; acetone;