(2S,4R,6R,7S,10R)-2,4-Bis-benzyloxymethyl-7-isopropyl-10-methyl-1,5-dioxa-spiro[5.5]undecane

Base Information

Chemical Name:(2S,4R,6R,7S,10R)-2,4-Bis-benzyloxymethyl-7-isopropyl-10-methyl-1,5-dioxa-spiro[5.5]undecane
CAS No.:122040-24-8
Molecular Formula:C₂₉H₄₀O₄
Molecular Weight:452.634
Hs Code.:

Synonyms:(2S,4R,6R,7S,10R)-2,4-Bis-benzyloxymethyl-7-isopropyl-10-methyl-1,5-dioxa-spiro[5.5]undecane

Suppliers and Price of (2S,4R,6R,7S,10R)-2,4-Bis-benzyloxymethyl-7-isopropyl-10-methyl-1,5-dioxa-spiro[5.5]undecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,4R,6R,7S,10R)-2,4-Bis-benzyloxymethyl-7-isopropyl-10-methyl-1,5-dioxa-spiro[5.5]undecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,4R,6R,7S,10R)-2,4-Bis-benzyloxymethyl-7-isopropyl-10-methyl-1,5-dioxa-spiro[5.5]undecane

There total 5 articles about (2S,4R,6R,7S,10R)-2,4-Bis-benzyloxymethyl-7-isopropyl-10-methyl-1,5-dioxa-spiro[5.5]undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 10458-14-7,14073-97-3,17627-49-5,7786-64-3
(2R,5S)-menthone

: 122040-19-1,122040-36-2
C₂₅H₄₀O₄Si₂

: 122040-24-8
(2S,4R,6R,7S,10R)-2,4-Bis-benzyloxymethyl-7-isopropyl-10-methyl-1,5-dioxa-spiro[5.5]undecane

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 6h;
DOI:10.1016/0040-4039(88)85095-0

Reference yield:

: 60656-87-3
benzyloxyacetoaldehyde

: 122040-24-8
(2S,4R,6R,7S,10R)-2,4-Bis-benzyloxymethyl-7-isopropyl-10-methyl-1,5-dioxa-spiro[5.5]undecane

Guidance literature:: Multi-step reaction with 5 steps

2: MCPBA

4: TMSOTf

5: 86 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 6 h / 0 °C

With trimethylsilyl trifluoromethanesulfonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/0040-4039(88)85095-0

Reference yield:

: 58931-16-1
1-(benzyloxy)-4-penten-2-ol

: 122040-24-8
(2S,4R,6R,7S,10R)-2,4-Bis-benzyloxymethyl-7-isopropyl-10-methyl-1,5-dioxa-spiro[5.5]undecane

Guidance literature:: Multi-step reaction with 4 steps

1: MCPBA

3: TMSOTf

4: 86 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 6 h / 0 °C

With trimethylsilyl trifluoromethanesulfonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/0040-4039(88)85095-0