(3S,4S)-N-isopentyl-3,4-bispyrrolidine

Base Information

• Chemical Name: (3S,4S)-N-isopentyl-3,4-bispyrrolidine
• CAS No.: 87974-33-2
• Molecular Formula: C₃₇H₄₅NO₆P₂
• Molecular Weight: 661.715
• Mol file: 87974-33-2.mol

Synonyms:(3S,4S)-N-isopentyl-3,4-bispyrrolidine

Chemical Property of (3S,4S)-N-isopentyl-3,4-bispyrrolidine

Chemical Property:

Purity/Quality:

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Technology Process of (3S,4S)-N-isopentyl-3,4-bispyrrolidine

There total 1 articles about (3S,4S)-N-isopentyl-3,4-bispyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

chlorobis(4-methoxyphenyl)phosphane (13685-30-8) + (3S,4S)-1-isopentyl-3,4-pyrrolidinediol (87974-35-4) → (3S,4S)-N-isopentyl-3,4-bispyrrolidine (87974-33-2)

Guidance literature:

With triethylamine;

DOI:10.1246/bcsj.57.823

Reference yield: 69.0%

rhodium(I)-bis(1,5-cyclooctadiene) tetrafluoroborate + (3S,4S)-N-isopentyl-3,4-bispyrrolidine (87974-33-2) → [Rh((CH3)2CHCH2CH2NH(CH2CHOP(C6H4OCH3)2)2)(C8H12)](2+)*BF4(1-)*ClO4(1-)

Guidance literature:

With perchloric acid; In ethanol; to soln. of reagents in EtOH HClO4 added as EtOH soln., stirred for 5 min at 0°C; cooled to -20°C, crystals filtered under N2, dried in vac.;

DOI:10.1246/bcsj.57.823

upstream raw materials:

chlorobis(4-methoxyphenyl)phosphane

(3S,4S)-1-isopentyl-3,4-pyrrolidinediol