methyl (S)-2-{[(benzyloxy)carbonyl](tert-butoxycarbonyl)amino}-3-{[bis(tert-butoxycarbonyl)amino]oxy}propanoate

Base Information

Chemical Name:methyl (S)-2-{[(benzyloxy)carbonyl](tert-butoxycarbonyl)amino}-3-{[bis(tert-butoxycarbonyl)amino]oxy}propanoate
CAS No.:1427803-64-2
Molecular Formula:C₂₇H₄₀N₂O₁₁
Molecular Weight:568.621
Hs Code.:

Synonyms:methyl (S)-2-{[(benzyloxy)carbonyl](tert-butoxycarbonyl)amino}-3-{[bis(tert-butoxycarbonyl)amino]oxy}propanoate

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Chemical Property of methyl (S)-2-{[(benzyloxy)carbonyl](tert-butoxycarbonyl)amino}-3-{[bis(tert-butoxycarbonyl)amino]oxy}propanoate

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Technology Process of methyl (S)-2-{[(benzyloxy)carbonyl](tert-butoxycarbonyl)amino}-3-{[bis(tert-butoxycarbonyl)amino]oxy}propanoate

There total 4 articles about methyl (S)-2-{[(benzyloxy)carbonyl](tert-butoxycarbonyl)amino}-3-{[bis(tert-butoxycarbonyl)amino]oxy}propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1067639-93-3
3-{[(1,1-dimethylethoxy)carbonyl]aminooxy}-N-[(phenylmethoxy)carbonyl]-L-serine methyl ester

: 24424-99-5
di-tert-butyl dicarbonate

: 1427803-63-1
methyl (S)-2-{[(benzyloxy)carbonyl]amino}-3-{[bis(tert-butoxycarbonyl)amino]oxy}propanoate

: 1427803-64-2
methyl (S)-2-{[(benzyloxy)carbonyl](tert-butoxycarbonyl)amino}-3-{[bis(tert-butoxycarbonyl)amino]oxy}propanoate

Guidance literature:: With dmap; In tetrahydrofuran; at 20 ℃; for 17h;
DOI:10.1055/s-0032-1317689

Reference yield:

: C₁₃H₁₉N₃O₅

: 1427803-64-2
methyl (S)-2-{[(benzyloxy)carbonyl](tert-butoxycarbonyl)amino}-3-{[bis(tert-butoxycarbonyl)amino]oxy}propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran

2: dmap / tetrahydrofuran / 17 h / 20 °C

With dmap; triethylamine; In tetrahydrofuran;
DOI:10.1055/s-0032-1317689

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1427803-64-2
methyl (S)-2-{[(benzyloxy)carbonyl](tert-butoxycarbonyl)amino}-3-{[bis(tert-butoxycarbonyl)amino]oxy}propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / 20 °C

2: dichloromethane

3: triethylamine / tetrahydrofuran

4: dmap / tetrahydrofuran / 17 h / 20 °C

With dmap; sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-0032-1317689