C₁₉H₁₃NOS

Base Information

• Chemical Name: C₁₉H₁₃NOS
• CAS No.: 1394964-99-8
• Molecular Formula: C₁₉H₁₃NOS
• Molecular Weight: 303.384
• Mol file: 1394964-99-8.mol

Synonyms:C₁₉H₁₃NOS

Chemical Property of C₁₉H₁₃NOS

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₁₉H₁₃NOS

There total 1 articles about C₁₉H₁₃NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

benzoic acid methyl ester (93-58-3,5705-52-2,80226-58-0) + 2-methylnaphtho[2,1-d]thiazole (20686-62-8) → C19H13NOS (1394964-99-8)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 24h; Reflux;

DOI:10.1021/ol302179r

Reference yield: 91.0%

triphenylborane (960-71-4) + C19H13NOS (1394964-99-8) → C31H22BNOS (1394979-79-3)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ol302179r

Reference yield: 75.0%

C19H13NOS (1394964-99-8) → C19H12BF2NOS (1394979-72-6)

Guidance literature:

With boron trifluoride diethyl etherate; triethylamine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/ol302179r

upstream raw materials:

benzoic acid methyl ester

2-methylnaphtho[2,1-d]thiazole

Downstream raw materials:

C₁₉H₁₂BF₂NOS

C₃₁H₂₂BNOS