C₁₃H₁₁NO

Base Information

• Chemical Name: C₁₃H₁₁NO
• CAS No.: 1562565-54-1
• Molecular Formula: C₁₃H₁₁NO
• Molecular Weight: 197.236

Synonyms:C₁₃H₁₁NO

Chemical Property of C₁₃H₁₁NO

Chemical Property:

Purity/Quality:

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Technology Process of C₁₃H₁₁NO

There total 2 articles about C₁₃H₁₁NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C16H19NOSi (1562568-59-5) → C13H11NO (1562565-54-1)

Guidance literature:

With potassium fluoride dihydrate; In methanol; at 20 ℃; for 3h;

DOI:10.1021/ol5002347

Reference yield:

C11H8INO → C13H11NO (1562565-54-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium cyanotrihydridoborate / 12 h / 0 - 20 °C / Inert atmosphere

2.1: [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); copper (I) iodide; triethylamine / 0.08 h / Inert atmosphere

2.2: 12 h / 20 °C / Inert atmosphere

3.1: potassium fluoride / methanol / 3 h / 20 °C / Inert atmosphere

With [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); potassium fluoride; copper (I) iodide; sodium cyanotrihydridoborate; triethylamine; In methanol;

DOI:10.1039/d2cc01169g

Reference yield: 95.0%

4-toluenesulfonyl azide (941-55-9) + C13H11NO (1562565-54-1) → 4-(furan-2-ylmethyl)-3-tosyl-3,4-dihydro-[1,2,3]triazolo[4,5-b]indole (1562569-65-6)

Guidance literature:

With triethylamine; copper(l) chloride; In acetonitrile; at 20 ℃; for 3h; regioselective reaction; Inert atmosphere; Schlenk technique;

DOI:10.1021/ol5002347

upstream raw materials:

C₁₆H₁₉NOSi

Downstream raw materials:

4-(furan-2-ylmethyl)-3-tosyl-3,4-dihydro-[1,2,3]triazolo[4,5-b]indole

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