1,8-bis-(benzyloxycarbonylmethyl)-4-(4'-nitrobenzyl)-1,4,8,11-tetraazacyclotetradecane

Base Information

Chemical Name:1,8-bis-(benzyloxycarbonylmethyl)-4-(4'-nitrobenzyl)-1,4,8,11-tetraazacyclotetradecane
CAS No.:1331909-96-6
Molecular Formula:C₃₅H₄₅N₅O₆
Molecular Weight:631.772
Hs Code.:

Synonyms:1,8-bis-(benzyloxycarbonylmethyl)-4-(4'-nitrobenzyl)-1,4,8,11-tetraazacyclotetradecane

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Chemical Property of 1,8-bis-(benzyloxycarbonylmethyl)-4-(4'-nitrobenzyl)-1,4,8,11-tetraazacyclotetradecane

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Technology Process of 1,8-bis-(benzyloxycarbonylmethyl)-4-(4'-nitrobenzyl)-1,4,8,11-tetraazacyclotetradecane

There total 4 articles about 1,8-bis-(benzyloxycarbonylmethyl)-4-(4'-nitrobenzyl)-1,4,8,11-tetraazacyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1264659-72-4
1,8-bis-(benzyloxycarbonylmethyl)-1,4,8,11-tetraazacyclotetradecane

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 1331909-96-6
1,8-bis-(benzyloxycarbonylmethyl)-4-(4'-nitrobenzyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: With triethylamine; In chloroform; at 20 ℃; for 10h;

Reference yield:

: 5437-45-6
Benzyl bromoacetate

: 1331909-96-6
1,8-bis-(benzyloxycarbonylmethyl)-4-(4'-nitrobenzyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 24 h / 20 °C

2: sodium hydroxide / 3 h

3: triethylamine / chloroform / 10 h / 20 °C

With triethylamine; sodium hydroxide; In chloroform; acetonitrile;

Reference yield:

: 75920-10-4
1,4,8,11-tetraazatricyclo[9.3.1.14,8]hexadecane

: 1331909-96-6
1,8-bis-(benzyloxycarbonylmethyl)-4-(4'-nitrobenzyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 24 h / 20 °C

2: sodium hydroxide / 3 h

3: triethylamine / chloroform / 10 h / 20 °C

With triethylamine; sodium hydroxide; In chloroform; acetonitrile;