Technology Process of C19H16F3NO2S
There total 4 articles about C19H16F3NO2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
manganese(IV) oxide;
In
toluene;
at 60 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/jo302052m
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: magnesium sulfate; toluene-4-sulfonic acid / dichloromethane / 0.17 h / 40 °C / Inert atmosphere
1.2: 40 °C / Inert atmosphere
2.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 20 °C / Inert atmosphere
3.1: manganese(IV) oxide / toluene / 2 h / 60 °C / Inert atmosphere
With
manganese(IV) oxide; trimethylsilyl trifluoromethanesulfonate; magnesium sulfate; toluene-4-sulfonic acid;
In
dichloromethane; toluene;
DOI:10.1021/jo302052m
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetonitrile / 16 h / Reflux
2.1: magnesium sulfate; toluene-4-sulfonic acid / dichloromethane / 0.17 h / 40 °C / Inert atmosphere
2.2: 40 °C / Inert atmosphere
3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 20 °C / Inert atmosphere
4.1: manganese(IV) oxide / toluene / 2 h / 60 °C / Inert atmosphere
With
manganese(IV) oxide; trimethylsilyl trifluoromethanesulfonate; magnesium sulfate; toluene-4-sulfonic acid;
In
dichloromethane; toluene; acetonitrile;
DOI:10.1021/jo302052m