4-acetoxyimino-5-(p-benzyloxyphenyl)-5-hydroxyhexanoic acid benzylamide

Base Information

Chemical Name:4-acetoxyimino-5-(p-benzyloxyphenyl)-5-hydroxyhexanoic acid benzylamide
CAS No.:134734-48-8
Molecular Formula:C₂₈H₃₀N₂O₅
Molecular Weight:474.557
Hs Code.:

Synonyms:4-acetoxyimino-5-(p-benzyloxyphenyl)-5-hydroxyhexanoic acid benzylamide

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Chemical Property of 4-acetoxyimino-5-(p-benzyloxyphenyl)-5-hydroxyhexanoic acid benzylamide

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Technology Process of 4-acetoxyimino-5-(p-benzyloxyphenyl)-5-hydroxyhexanoic acid benzylamide

There total 5 articles about 4-acetoxyimino-5-(p-benzyloxyphenyl)-5-hydroxyhexanoic acid benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 108-24-7
acetic anhydride

: 134734-46-6
5(p-benzyloxyphenyl)-5-hydroxy-4-hydroxyliminohexanoic acid benzylamide

: 134734-48-8
4-acetoxyimino-5-(p-benzyloxyphenyl)-5-hydroxyhexanoic acid benzylamide

Guidance literature:: With dmap; In pyridine; dichloromethane; Ambient temperature;
DOI:10.1002/jhet.5570280311

Reference yield:

: 106281-27-0
2-(p-benzyloxyphenyl)-6-hydroxy-2-methyl-2H-pyran-3(6H)-one

: 134734-48-8
4-acetoxyimino-5-(p-benzyloxyphenyl)-5-hydroxyhexanoic acid benzylamide

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / CrO₃, conc. H₂SO₄, H₂O (Jones reagent) / acetone / 0.25 h

2: 95 percent / zinc dust / CHCl₃; acetic acid / 3 h / Ambient temperature

3: 82 percent / KCN / methanol / 55 °C

4: 94 percent / hydroxylamine hydrochloride, NaOAc * 3H₂O / methanol / 55 °C

5: 95 percent / DMAP / CH₂Cl₂; pyridine / Ambient temperature

With chromium(VI) oxide; dmap; potassium cyanide; sulfuric acid; hydroxylamine hydrochloride; water; sodium acetate; zinc; In pyridine; methanol; dichloromethane; chloroform; acetic acid; acetone;
DOI:10.1002/jhet.5570280311

Reference yield:

: 134734-37-5
δ-(p-benzyloxyxyphenyl)-δ-methyl-δ-(γ-oxo)crotonolactone

: 134734-48-8
4-acetoxyimino-5-(p-benzyloxyphenyl)-5-hydroxyhexanoic acid benzylamide

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / zinc dust / CHCl₃; acetic acid / 3 h / Ambient temperature

2: 82 percent / KCN / methanol / 55 °C

3: 94 percent / hydroxylamine hydrochloride, NaOAc * 3H₂O / methanol / 55 °C

4: 95 percent / DMAP / CH₂Cl₂; pyridine / Ambient temperature

With dmap; potassium cyanide; hydroxylamine hydrochloride; sodium acetate; zinc; In pyridine; methanol; dichloromethane; chloroform; acetic acid;
DOI:10.1002/jhet.5570280311