5(p-benzyloxyphenyl)-5-hydroxy-4-hydroxyliminohexanoic acid benzylamide

Base Information

Chemical Name:5(p-benzyloxyphenyl)-5-hydroxy-4-hydroxyliminohexanoic acid benzylamide
CAS No.:134734-46-6
Molecular Formula:C₂₆H₂₈N₂O₄
Molecular Weight:432.519
Hs Code.:

Synonyms:5(p-benzyloxyphenyl)-5-hydroxy-4-hydroxyliminohexanoic acid benzylamide

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Chemical Property of 5(p-benzyloxyphenyl)-5-hydroxy-4-hydroxyliminohexanoic acid benzylamide

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Technology Process of 5(p-benzyloxyphenyl)-5-hydroxy-4-hydroxyliminohexanoic acid benzylamide

There total 4 articles about 5(p-benzyloxyphenyl)-5-hydroxy-4-hydroxyliminohexanoic acid benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 134734-44-4
5-(p-benzyloxyphenyl)-5-hydroxy-4-oxohexanoic acid benzylamide

: 134734-46-6
5(p-benzyloxyphenyl)-5-hydroxy-4-hydroxyliminohexanoic acid benzylamide

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In methanol; at 55 ℃;
DOI:10.1002/jhet.5570280311

Reference yield:

: 106281-27-0
2-(p-benzyloxyphenyl)-6-hydroxy-2-methyl-2H-pyran-3(6H)-one

: 134734-46-6
5(p-benzyloxyphenyl)-5-hydroxy-4-hydroxyliminohexanoic acid benzylamide

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / CrO₃, conc. H₂SO₄, H₂O (Jones reagent) / acetone / 0.25 h

2: 95 percent / zinc dust / CHCl₃; acetic acid / 3 h / Ambient temperature

3: 82 percent / KCN / methanol / 55 °C

4: 94 percent / hydroxylamine hydrochloride, NaOAc * 3H₂O / methanol / 55 °C

With chromium(VI) oxide; potassium cyanide; sulfuric acid; hydroxylamine hydrochloride; water; sodium acetate; zinc; In methanol; chloroform; acetic acid; acetone;
DOI:10.1002/jhet.5570280311

Reference yield:

: 134734-37-5
δ-(p-benzyloxyxyphenyl)-δ-methyl-δ-(γ-oxo)crotonolactone

: 134734-46-6
5(p-benzyloxyphenyl)-5-hydroxy-4-hydroxyliminohexanoic acid benzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / zinc dust / CHCl₃; acetic acid / 3 h / Ambient temperature

2: 82 percent / KCN / methanol / 55 °C

3: 94 percent / hydroxylamine hydrochloride, NaOAc * 3H₂O / methanol / 55 °C

With potassium cyanide; hydroxylamine hydrochloride; sodium acetate; zinc; In methanol; chloroform; acetic acid;
DOI:10.1002/jhet.5570280311