C₂₉H₄₈N₂O₈Si

Base Information

Chemical Name:C₂₉H₄₈N₂O₈Si
CAS No.:1407508-26-2
Molecular Formula:C₂₉H₄₈N₂O₈Si
Molecular Weight:580.794
Hs Code.:

C<sub>29</sub>H<sub>48</sub>N<sub>2</sub>O<sub>8</sub>Si

Synonyms:C₂₉H₄₈N₂O₈Si

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Chemical Property of C₂₉H₄₈N₂O₈Si

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Technology Process of C₂₉H₄₈N₂O₈Si

There total 8 articles about C₂₉H₄₈N₂O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1407508-25-1
C₁₆H₃₅NO₅Si

: 1148-11-4
N-Benzyloxycarbonyl-L-proline

: 1407508-26-2
C₂₉H₄₈N₂O₈Si

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetasy.2012.08.008

Reference yield:

: 626201-36-3
(2R,3R,5R,6R)-5,6-dimethoxy-5,6-dimethyl-1,4-dioxane-2,3-dicarbothioic acid di-S-ethyl ester

: 1407508-26-2
C₂₉H₄₈N₂O₈Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.25 h / -78 °C

1.3: 0 - 20 °C

2.1: titanium(IV) isopropylate / 240 h / 100 °C / Inert atmosphere; Sealed tube

3.1: lithium aluminium tetrahydride / 70 °C

4.1: sodium hydride / tetrahydrofuran; pentane / 20 °C

4.2: 20 °C

5.1: di-isopropyl azodicarboxylate; triphenylphosphine; hydrogen azide / tetrahydrofuran; benzene / 0 - 20 °C / Inert atmosphere

6.1: hydrogen; 10% Pd/C / ethyl acetate; ethanol / 3 h / 2585.81 Torr

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; benzotriazol-1-ol / dichloromethane / 0 - 20 °C / Inert atmosphere

With titanium(IV) isopropylate; lithium aluminium tetrahydride; hydrogen azide; di-isopropyl azodicarboxylate; 10% Pd/C; hydrogen; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; ethyl acetate; pentane; benzene; 5.1: |Mitsunobu Displacement;
DOI:10.1016/j.tetasy.2012.08.008

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1407508-26-2
C₂₉H₄₈N₂O₈Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; pentane / 20 °C

1.2: 20 °C

2.1: di-isopropyl azodicarboxylate; triphenylphosphine; hydrogen azide / tetrahydrofuran; benzene / 0 - 20 °C / Inert atmosphere

3.1: hydrogen; 10% Pd/C / ethyl acetate; ethanol / 3 h / 2585.81 Torr

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; benzotriazol-1-ol / dichloromethane / 0 - 20 °C / Inert atmosphere

With hydrogen azide; di-isopropyl azodicarboxylate; 10% Pd/C; hydrogen; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; pentane; benzene; 2.1: |Mitsunobu Displacement;
DOI:10.1016/j.tetasy.2012.08.008