4,6-Bis(tert-butyldimethylsilyloxy)-1,2,3,6-tetrahydro-6-methyl-2-(4-nitrophenyl)-1-pyridazincarbonitril

Base Information

Chemical Name:4,6-Bis(tert-butyldimethylsilyloxy)-1,2,3,6-tetrahydro-6-methyl-2-(4-nitrophenyl)-1-pyridazincarbonitril
CAS No.:108946-48-1
Molecular Formula:C₂₄H₄₀N₄O₄Si₂
Molecular Weight:504.777
Hs Code.:

Synonyms:4,6-Bis(tert-butyldimethylsilyloxy)-1,2,3,6-tetrahydro-6-methyl-2-(4-nitrophenyl)-1-pyridazincarbonitril

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Chemical Property of 4,6-Bis(tert-butyldimethylsilyloxy)-1,2,3,6-tetrahydro-6-methyl-2-(4-nitrophenyl)-1-pyridazincarbonitril

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Technology Process of 4,6-Bis(tert-butyldimethylsilyloxy)-1,2,3,6-tetrahydro-6-methyl-2-(4-nitrophenyl)-1-pyridazincarbonitril

There total 3 articles about 4,6-Bis(tert-butyldimethylsilyloxy)-1,2,3,6-tetrahydro-6-methyl-2-(4-nitrophenyl)-1-pyridazincarbonitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 108946-44-7
2,4-bis(tert-butyldimethylsilyloxy)-1,3-pentadiene

: 58468-75-0
(4-nitro-phenyl)-cis-diazenecarbonitrile

: 108946-48-1
4,6-Bis(tert-butyldimethylsilyloxy)-1,2,3,6-tetrahydro-6-methyl-2-(4-nitrophenyl)-1-pyridazincarbonitril

Guidance literature:: In chloroform; for 2h; Ambient temperature;

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 108946-48-1
4,6-Bis(tert-butyldimethylsilyloxy)-1,2,3,6-tetrahydro-6-methyl-2-(4-nitrophenyl)-1-pyridazincarbonitril

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / NEt₃ / diethyl ether / 0.33 h / Ambient temperature

2: 74 percent / CHCl₃ / 2 h / Ambient temperature

With triethylamine; In diethyl ether; chloroform;

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 108946-48-1
4,6-Bis(tert-butyldimethylsilyloxy)-1,2,3,6-tetrahydro-6-methyl-2-(4-nitrophenyl)-1-pyridazincarbonitril

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / NEt₃ / diethyl ether / 0.33 h / Ambient temperature

2: 74 percent / CHCl₃ / 2 h / Ambient temperature

With triethylamine; In diethyl ether; chloroform;