12c-methanesulfinyl-p-tolyl-12-propyl-12,12c-dihydro-4,8-dioxa-12-aza-dibenzo[cd,mn]pyrene

Base Information

• Chemical Name: 12c-methanesulfinyl-p-tolyl-12-propyl-12,12c-dihydro-4,8-dioxa-12-aza-dibenzo[cd,mn]pyrene
• CAS No.: 906377-55-7
• Molecular Formula: C₃₀H₂₅NO₃S
• Molecular Weight: 479.599

Synonyms:12c-methanesulfinyl-p-tolyl-12-propyl-12,12c-dihydro-4,8-dioxa-12-aza-dibenzo[cd,mn]pyrene

Chemical Property of 12c-methanesulfinyl-p-tolyl-12-propyl-12,12c-dihydro-4,8-dioxa-12-aza-dibenzo[cd,mn]pyrene

Chemical Property:

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Technology Process of 12c-methanesulfinyl-p-tolyl-12-propyl-12,12c-dihydro-4,8-dioxa-12-aza-dibenzo[cd,mn]pyrene

There total 1 articles about 12c-methanesulfinyl-p-tolyl-12-propyl-12,12c-dihydro-4,8-dioxa-12-aza-dibenzo[cd,mn]pyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

C22H16NO2(1+)*F6P(1-) + Methyl p-tolyl sulfoxide (934-72-5) → 12c-methanesulfinyl-p-tolyl-12-propyl-12,12c-dihydro-4,8-dioxa-12-aza-dibenzo[cd,mn]pyrene (906377-55-7)

Guidance literature:

Methyl p-tolyl sulfoxide; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h;

C₂₂H₁₆NO₂⁽¹⁺⁾*F₆P^(1-); In tetrahydrofuran; hexane; at 0 - 20 ℃; for 14h; Further stages.;

DOI:10.1039/b605187a

Reference yield:

12c-methanesulfinyl-p-tolyl-12-propyl-12,12c-dihydro-4,8-dioxa-12-aza-dibenzo[cd,mn]pyrene (906377-55-7) + trifluoroacetic anhydride (407-25-0) → C32H24F3NO4S + C2F3O2(1-)*C22H16NO2(1+) (906377-60-4)

Guidance literature:

In dichloromethane; at 20 ℃; for 0.333333h; Title compound not separated from byproducts.;

DOI:10.1039/b605187a

upstream raw materials:

Methyl p-tolyl sulfoxide

Downstream raw materials:

C₂F₃O₂^(1-)*C₂₂H₁₆NO₂⁽¹⁺⁾

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