naphthalen-2-yl phenylmethanesulfonate

Base Information

• Chemical Name: naphthalen-2-yl phenylmethanesulfonate
• CAS No.: 15161-08-7
• Molecular Formula: C₁₇H₁₄O₃S
• Molecular Weight: 298.362
• Mol file: 15161-08-7.mol

Synonyms:naphthalen-2-yl phenylmethanesulfonate

Chemical Property of naphthalen-2-yl phenylmethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of naphthalen-2-yl phenylmethanesulfonate

There total 3 articles about naphthalen-2-yl phenylmethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

β-naphthol (135-19-3) + benzenesulfonyl chloride (1939-99-7) → naphthalen-2-yl phenylmethanesulfonate (15161-08-7)

Guidance literature:

With sodium hydroxide;

Reference yield:

phenylmethanethiol (100-53-8) → naphthalen-2-yl phenylmethanesulfonate (15161-08-7)

Guidance literature:

Multi-step reaction with 2 steps

1: dihydrogen peroxide; trichlorophosphate / water; acetonitrile / 25 °C

2: Amberlite IRA-400 OH^(1-)-form / water; acetonitrile / 0.03 h / 25 °C

With dihydrogen peroxide; trichlorophosphate; In water; acetonitrile;

DOI:10.1016/j.tet.2012.04.040

Reference yield:

→ naphthalen-2-yl phenylmethanesulfonate (15161-08-7)

Guidance literature:

Entspr. RSO2Cl, R'OH;

upstream raw materials:

β-naphthol

benzenesulfonyl chloride

phenylmethanethiol

Refernces