C₂₆H₃₂FNO₄SSi

Base Information Edit

Chemical Name:C₂₆H₃₂FNO₄SSi
CAS No.:1374232-95-7
Molecular Formula:C₂₆H₃₂FNO₄SSi
Molecular Weight:501.694
Hs Code.:
Mol file:1374232-95-7.mol

C<sub>26</sub>H<sub>32</sub>FNO<sub>4</sub>SSi

Synonyms:C₂₆H₃₂FNO₄SSi

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Chemical Property of C₂₆H₃₂FNO₄SSi Edit

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Technology Process of C₂₆H₃₂FNO₄SSi

There total 9 articles about C₂₆H₃₂FNO₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 766-98-3
1-ethynyl-4-fluorobenzene

: 1374232-94-6
C₁₈H₂₈BrNO₄SSi

: 1374232-95-7
C₂₆H₃₂FNO₄SSi

Guidance literature:: With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine; In N,N-dimethyl-formamide; at 80 ℃; Inert atmosphere;

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 1374232-95-7
C₂₆H₃₂FNO₄SSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: copper(l) iodide; copper diacetate / water / 48 h / 100 °C

2.1: polyphosphoric acid / 3 h / 90 °C

3.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C

4.2: 0 - 20 °C

5.1: diethylzinc / hexane; toluene / 0 - 20 °C

6.1: N-Bromosuccinimide / dichloromethane / 1 h / 0 - 20 °C

7.1: boron tribromide / dichloromethane / 1 h / -20 - 0 °C

7.2: Cooling with ice

8.1: triethylamine / dmap / tetrahydrofuran / 10 h / 0 - 20 °C

9.1: piperidine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

With piperidine; N-Bromosuccinimide; n-butyllithium; diethylzinc; boron tribromide; triethylamine; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine; copper diacetate; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 879-56-1
7-Methoxy-2,3-dihydro-1H-quinolin-4-one

: 1374232-95-7
C₂₆H₃₂FNO₄SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C

2.2: 0 - 20 °C

3.1: diethylzinc / hexane; toluene / 0 - 20 °C

4.1: N-Bromosuccinimide / dichloromethane / 1 h / 0 - 20 °C

5.1: boron tribromide / dichloromethane / 1 h / -20 - 0 °C

5.2: Cooling with ice

6.1: triethylamine / dmap / tetrahydrofuran / 10 h / 0 - 20 °C

7.1: piperidine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

With piperidine; N-Bromosuccinimide; n-butyllithium; diethylzinc; boron tribromide; triethylamine; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;