(4S,5R,6R)-(-)-5-benzyloxy-6-(3-benzyloxypropyl)-4-[(R)-hydroxy-(phenyl)methyl]-2,2-dimethyl-1,3-dioxan

Base Information

Chemical Name:(4S,5R,6R)-(-)-5-benzyloxy-6-(3-benzyloxypropyl)-4-[(R)-hydroxy-(phenyl)methyl]-2,2-dimethyl-1,3-dioxan
CAS No.:1032514-47-8
Molecular Formula:C₃₀H₃₆O₅
Molecular Weight:476.613
Hs Code.:

Synonyms:(4S,5R,6R)-(-)-5-benzyloxy-6-(3-benzyloxypropyl)-4-[(R)-hydroxy-(phenyl)methyl]-2,2-dimethyl-1,3-dioxan

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Chemical Property of (4S,5R,6R)-(-)-5-benzyloxy-6-(3-benzyloxypropyl)-4-[(R)-hydroxy-(phenyl)methyl]-2,2-dimethyl-1,3-dioxan

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Technology Process of (4S,5R,6R)-(-)-5-benzyloxy-6-(3-benzyloxypropyl)-4-[(R)-hydroxy-(phenyl)methyl]-2,2-dimethyl-1,3-dioxan

There total 1 articles about (4S,5R,6R)-(-)-5-benzyloxy-6-(3-benzyloxypropyl)-4-[(R)-hydroxy-(phenyl)methyl]-2,2-dimethyl-1,3-dioxan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1032514-45-6
(4R,5R,6R)-(-)-5-benzyloxy-6-(3-benzyloxypropyl)-4-[(R)-(tert-butyldimethylsilyloxy)(phenyl)methyl]-2,2-dimethyl-1,3-dioxan

: 1032514-47-8
(4S,5R,6R)-(-)-5-benzyloxy-6-(3-benzyloxypropyl)-4-[(R)-hydroxy-(phenyl)methyl]-2,2-dimethyl-1,3-dioxan

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/chem.200701647

Reference yield: 36.0%

: 1032514-47-8
(4S,5R,6R)-(-)-5-benzyloxy-6-(3-benzyloxypropyl)-4-[(R)-hydroxy-(phenyl)methyl]-2,2-dimethyl-1,3-dioxan

: 77-76-9
2,2-dimethoxy-propane

: 1032514-49-0
(1R,2R)-(-)-1,5-dibenzyloxy-1-[(4R,5R)-2,2-dimethyl-5-phenyl-1,3-dioxolan-4-yl]pentan-2-ol

Guidance literature:: (4S,5R,6R)-(-)-5-benzyloxy-6-(3-benzyloxypropyl)-4-[(R)-hydroxy-(phenyl)methyl]-2,2-dimethyl-1,3-dioxan; With toluene-4-sulfonic acid; In acetone; at 20 ℃; for 24h;

2,2-dimethoxy-propane; With pyridinium p-toluenesulfonate; In acetone; at 20 ℃; for 1h;
DOI:10.1002/chem.200701647