Technology Process of C41H46O14S
There total 8 articles about C41H46O14S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1: Na(1+)*HSO4(1-)*SiO2 = NaHSO4*SiO2 / acetonitrile; N,N-dimethyl-formamide / 2 h / 20 °C
2: pyridine / dichloromethane / 2.5 h / 20 °C
3: dmap; triethylamine / dichloromethane / 20 °C
4: sodium formate; methanol / ethyl acetate / 24 h / 70 °C
5: sodium hydride / N,N-dimethyl-formamide / 0 °C
With
pyridine; methanol; dmap; Na(1+)*HSO4(1-)*SiO2 = NaHSO4*SiO2; sodium formate; sodium hydride; triethylamine;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1080/10286020.2013.863185
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap; triethylamine / dichloromethane / 20 °C
2: sodium formate; methanol / ethyl acetate / 24 h / 70 °C
3: sodium hydride / N,N-dimethyl-formamide / 0 °C
With
methanol; dmap; sodium formate; sodium hydride; triethylamine;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1080/10286020.2013.863185