benzyl 2-acetamido-2-deoxy-3-O--6-O-methyl-α-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-2-deoxy-3-O--6-O-methyl-α-D-glucopyranoside
CAS No.:88574-10-1
Molecular Formula:C₂₀H₂₉NO₈
Molecular Weight:411.452
Hs Code.:

benzyl 2-acetamido-2-deoxy-3-O-<D-1-(methoxycarbonyl)ethyl>-6-O-methyl-α-D-glucopyranoside

Synonyms:benzyl 2-acetamido-2-deoxy-3-O--6-O-methyl-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-acetamido-2-deoxy-3-O--6-O-methyl-α-D-glucopyranoside

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Technology Process of benzyl 2-acetamido-2-deoxy-3-O--6-O-methyl-α-D-glucopyranoside

There total 1 articles about benzyl 2-acetamido-2-deoxy-3-O--6-O-methyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 909889-92-5
benzyl 2-acetamido-2-deoxy-3-O--α-D-glucopyranoside

: 74-88-4
methyl iodide

: 88574-10-1
benzyl 2-acetamido-2-deoxy-3-O--6-O-methyl-α-D-glucopyranoside

Guidance literature:: With silver(l) oxide; In 1,4-dioxane; Ambient temperature;
DOI:10.1016/0008-6215(83)88409-2

Reference yield:

: 88574-10-1
benzyl 2-acetamido-2-deoxy-3-O--6-O-methyl-α-D-glucopyranoside

: 88574-26-9
2-((2S,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-5-hydroxy-6-methoxymethyl-tetrahydro-pyran-4-yloxy)-propionic acid

Guidance literature:: With potassium hydroxide; Amberlite IR-120B (H⁽¹⁺⁾); In methanol; at 0 ℃; for 0.166667h;
DOI:10.1016/0008-6215(83)88409-2

Reference yield:

: 88574-10-1
benzyl 2-acetamido-2-deoxy-3-O--6-O-methyl-α-D-glucopyranoside

: 88574-13-4
N-<2-O-(benzyl 2-acetamido-2,3-dideoxy-6-O-methyl-α-D-glucopyranoside-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 0.5M aq. KOH, Amberlite IR-120B (H⁽¹⁺⁾) / methanol / 0.17 h / 0 °C

2: 1.) HOSu, DCC 2.) triethylamine / 1.) oxolane, 0 deg C, 1 h; 2.) r.t., 3 h

With potassium hydroxide; 1-hydroxy-pyrrolidine-2,5-dione; Amberlite IR-120B (H⁽¹⁺⁾); triethylamine; dicyclohexyl-carbodiimide; In methanol;
DOI:10.1016/0008-6215(83)88409-2