N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-β-D-riboside

Base Information

Chemical Name:N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-β-D-riboside
CAS No.:1256382-05-4
Molecular Formula:C₂₀H₃₂Cl₂N₂O₅
Molecular Weight:451.39
Hs Code.:

Synonyms:N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-β-D-riboside

Suppliers and Price of N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-β-D-riboside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-β-D-riboside

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-β-D-riboside

There total 5 articles about N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-β-D-riboside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
D-Ribose

: 1256381-59-5
N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamine

: N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-α-D-riboside

: 1256382-05-4
N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-β-D-riboside

Guidance literature:: With acetic acid; In methanol; at 40 ℃; for 3h; Capped vial;

Reference yield:

: 64977-05-5
4-(4-(N,N-bis(2-chloroethyl)amino)phenyl)butanal

: N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-α-D-riboside

: 1256382-05-4
N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-β-D-riboside

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / ethanol / 0.58 h

2: hydrogenchloride; triethylamine-borane / ethanol / 0 °C

3: acetic acid / methanol / 3 h / 40 °C / Capped vial

With hydrogenchloride; triethylamine-borane; acetic acid; triethylamine; In methanol; ethanol;

Reference yield:

: 305-03-3
chlorambucil

: N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-α-D-riboside

: 1256382-05-4
N-methoxy-4-(4-N',N'-bis(2-chloroethyl)amino)phenylbutylamino-β-D-riboside

Guidance literature:: Multi-step reaction with 5 steps

1: 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1.08 h / 0 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

3: triethylamine / ethanol / 0.58 h

4: hydrogenchloride; triethylamine-borane / ethanol / 0 °C

5: acetic acid / methanol / 3 h / 40 °C / Capped vial

With 4-methyl-morpholine; hydrogenchloride; lithium aluminium tetrahydride; triethylamine-borane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane;