1,1-Dichloro-1,2,2-trimethyl-2-phenyldisilane

Base Information

• Chemical Name: 1,1-Dichloro-1,2,2-trimethyl-2-phenyldisilane
• CAS No.: 114994-59-1
• Molecular Formula: C₉H₁₄Cl₂Si₂
• Molecular Weight: 249.287
• DSSTox Substance ID: DTXSID101251570
• Nikkaji Number: J2.443.141J

Synonyms:1,1-Dichloro-1,2,2-trimethyl-2-phenyldisilane;SCHEMBL10355215;DTXSID101251570;114994-59-1

Chemical Property of 1,1-Dichloro-1,2,2-trimethyl-2-phenyldisilane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 248.0011089
• Heavy Atom Count: 13
• Complexity: 175

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C[Si](C)(C1=CC=CC=C1)[Si](C)(Cl)Cl

Technology Process of 1,1-Dichloro-1,2,2-trimethyl-2-phenyldisilane

There total 3 articles about 1,1-Dichloro-1,2,2-trimethyl-2-phenyldisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1,1,2-trichloro-1,2,2-trimethyldisilane (13528-88-6) + phenylmagnesium bromide (100-58-3) → 1,1-dichloro-2-phenyl-1,2,2-trimethyldisilane (114994-59-1)

Guidance literature:

copper(l) iodide; In diethyl ether; for 12h; 0 deg C - r.t.;

DOI:10.1246/cl.1988.1883

Reference yield:

1,1,2-trichloro-1,2,2-trimethyldisilane (13528-88-6) + phenyllithium (591-51-5) → 1,1-dichloro-2-phenyl-1,2,2-trimethyldisilane (114994-59-1) + 1,2-dichloro-1-phenyl-1,2,2-trimethyldisilane (111544-68-4)

Guidance literature:

copper(l) iodide; In diethyl ether; Petroleum ether; for 12h; Yield given. Yields of byproduct given; 0 deg C - r.t.;

DOI:10.1246/cl.1988.1883

Reference yield:

1,1,2-trichloro-1,2,2-trimethyldisilane (13528-88-6) + phenylmagnesium bromide (100-58-3) → 1,1-dichloro-2-phenyl-1,2,2-trimethyldisilane (114994-59-1) + 1,2-dichloro-1-phenyl-1,2,2-trimethyldisilane (111544-68-4)

Guidance literature:

With CoCl₂; In diethyl ether; for 12h; 0 deg C - r.t.;

DOI:10.1246/cl.1988.1883

upstream raw materials:

1,1,2-trichloro-1,2,2-trimethyldisilane

phenylmagnesium bromide

phenyllithium

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