(S)-2-N-benzyl-N-[(S)-2-N-benzyl-N-{(S)-N-allyl-N-benzylaminopropyl}amino-3-methylbutyl]amino-4-methyl-pentan-1-ol

Base Information

• Chemical Name: (S)-2-N-benzyl-N-[(S)-2-N-benzyl-N-{(S)-N-allyl-N-benzylaminopropyl}amino-3-methylbutyl]amino-4-methyl-pentan-1-ol
• CAS No.: 717127-78-1
• Molecular Formula: C₃₈H₅₅N₃O
• Molecular Weight: 569.874

Synonyms:(S)-2-N-benzyl-N-[(S)-2-N-benzyl-N-{(S)-N-allyl-N-benzylaminopropyl}amino-3-methylbutyl]amino-4-methyl-pentan-1-ol

Chemical Property of (S)-2-N-benzyl-N-[(S)-2-N-benzyl-N-{(S)-N-allyl-N-benzylaminopropyl}amino-3-methylbutyl]amino-4-methyl-pentan-1-ol

Chemical Property:

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Technology Process of (S)-2-N-benzyl-N-[(S)-2-N-benzyl-N-{(S)-N-allyl-N-benzylaminopropyl}amino-3-methylbutyl]amino-4-methyl-pentan-1-ol

There total 2 articles about (S)-2-N-benzyl-N-[(S)-2-N-benzyl-N-{(S)-N-allyl-N-benzylaminopropyl}amino-3-methylbutyl]amino-4-methyl-pentan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzyl-L-leucine methyl ester (66399-70-0) → (S)-2-N-benzyl-N-[(S)-2-N-benzyl-N-{(S)-N-allyl-N-benzylaminopropyl}amino-3-methylbutyl]amino-4-methyl-pentan-1-ol (717127-78-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 56 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 0 - 20 °C

2: 115 mg / CH₂Cl₂ / 12 h / 20 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1039/b401447b

Reference yield:

(S)-4-methyl-[(phenylmethyl)amino]pentan-1-ol (10249-88-4) + Trifluoro-methanesulfonate(S)-1-[(S)-2-(allyl-benzyl-amino)-propyl]-1-benzyl-2-isopropyl-aziridinium; → (S)-2-N-benzyl-N-[(S)-2-N-benzyl-N-{(S)-N-allyl-N-benzylaminopropyl}amino-3-methylbutyl]amino-4-methyl-pentan-1-ol (717127-78-1)

Guidance literature:

In dichloromethane; at 20 ℃; for 12h;

DOI:10.1039/b401447b

Reference yield:

trifluoromethylsulfonic anhydride (358-23-6) + (S)-2-N-benzyl-N-[(S)-2-N-benzyl-N-{(S)-N-allyl-N-benzylaminopropyl}amino-3-methylbutyl]amino-4-methyl-pentan-1-ol (717127-78-1) → Trifluoro-methanesulfonate(S)-1-((S)-2-{[(S)-2-(allyl-benzyl-amino)-propyl]-benzyl-amino}-3-methyl-butyl)-1-benzyl-2-isobutyl-aziridinium;

Guidance literature:

With triethylamine; In dichloromethane; at -78 ℃; for 1h;

DOI:10.1039/b401447b

upstream raw materials:

(S)-4-methyl-[(phenylmethyl)amino]pentan-1-ol

N-benzyl-L-leucine methyl ester

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