C₂₃H₂₄N₂O₂

Base Information

Chemical Name:C₂₃H₂₄N₂O₂
CAS No.:655240-19-0
Molecular Formula:C₂₃H₂₄N₂O₂
Molecular Weight:360.456
Hs Code.:

C<sub>23</sub>H<sub>24</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₃H₂₄N₂O₂

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Chemical Property of C₂₃H₂₄N₂O₂

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Technology Process of C₂₃H₂₄N₂O₂

There total 8 articles about C₂₃H₂₄N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 655240-18-9
(1S,3R)-2-Benzyl-8-methoxy-1-(2-methoxycarbonyl-ethyl)-9-methyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid ethyl ester

: 655240-19-0
C₂₃H₂₄N₂O₂

Guidance literature:: (1S,3R)-2-Benzyl-8-methoxy-1-(2-methoxycarbonyl-ethyl)-9-methyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid ethyl ester; With sodium hydride; In methanol; toluene; Heating;

With potassium hydroxide; In 1,4-dioxane; Heating;
DOI:10.1021/ol0362212

Reference yield:

: 354574-31-5
2-iodo-6-methoxybenzenamine

: 655240-19-0
C₂₃H₂₄N₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: 75 percent / Pd(OAc)2; LiCl; K₂CO₃ / dimethylformamide / 36 h / 100 °C

2.1: NaH / dimethylformamide / 1.5 h / 0 °C

3.1: 1.69 g / aq. HCl / tetrahydrofuran / 0 - 20 °C

4.1: Na₂SO₄ / ethanol / 8 h / 0 °C

5.1: 8.64 g / NaBH₄; Na₂SO₄ / ethanol / -10 - 20 °C

6.1: AcOH / CH₂Cl₂ / 0 - 20 °C

7.1: NaH; MeOH / toluene / 5 h / Heating

7.2: 80 percent / aq. KOH / dioxane / 72 h / Heating

With hydrogenchloride; methanol; palladium diacetate; sodium tetrahydroborate; sodium hydride; potassium carbonate; acetic acid; sodium sulfate; lithium chloride; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; 6.1: Pictet-Spengler condensation / 7.1: Dieckmann cyclization;
DOI:10.1021/jo052081t

Reference yield:

: 655240-14-5
(5R,2S)-3,6-diethoxy-2-isopropyl-5-[7-methoxy-2-(triethylsilyl)-3-indolyl]methyl-2,5-dihydropyrazine

: 655240-19-0
C₂₃H₂₄N₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: NaH / dimethylformamide / 1.5 h / 0 °C

2.1: 1.69 g / aq. HCl / tetrahydrofuran / 0 - 20 °C

3.1: Na₂SO₄ / ethanol / 8 h / 0 °C

4.1: 8.64 g / NaBH₄; Na₂SO₄ / ethanol / -10 - 20 °C

5.1: AcOH / CH₂Cl₂ / 0 - 20 °C

6.1: NaH; MeOH / toluene / 5 h / Heating

6.2: 80 percent / aq. KOH / dioxane / 72 h / Heating

With hydrogenchloride; methanol; sodium tetrahydroborate; sodium hydride; acetic acid; sodium sulfate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; 5.1: Pictet-Spengler condensation / 6.1: Dieckmann cyclization;
DOI:10.1021/jo052081t