N-(L-phenylalanyl-L-leucyl)-β-D-glucopyranosylamine trifluoroacetate

Base Information

Chemical Name:N-(L-phenylalanyl-L-leucyl)-β-D-glucopyranosylamine trifluoroacetate
CAS No.:136860-12-3
Molecular Formula:C₂HF₃O₂*C₂₁H₃₃N₃O₇
Molecular Weight:553.533
Hs Code.:

Synonyms:N-(L-phenylalanyl-L-leucyl)-β-D-glucopyranosylamine trifluoroacetate

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Chemical Property of N-(L-phenylalanyl-L-leucyl)-β-D-glucopyranosylamine trifluoroacetate

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Technology Process of N-(L-phenylalanyl-L-leucyl)-β-D-glucopyranosylamine trifluoroacetate

There total 3 articles about N-(L-phenylalanyl-L-leucyl)-β-D-glucopyranosylamine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 136860-06-5
N--L-phenylalanyl-L-leucyl>-β-D-glucopyranosylamine

: 136860-12-3
N-(L-phenylalanyl-L-leucyl)-β-D-glucopyranosylamine trifluoroacetate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1002/hlca.19910740505

Reference yield:

: 7284-37-9,50444-86-5
D-glucopyranosyl amine

: 136860-12-3
N-(L-phenylalanyl-L-leucyl)-β-D-glucopyranosylamine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) isobutyl chloroformate, N-methylmorpholine / 1) THF, -15 deg C, 2 min, 2a) THF, H₂O, -15 deg C, 10 min, 2b) RT, overnight

2: 75 percent / CF₃CO₂H / CH₂Cl₂ / 0.5 h / Ambient temperature

With 4-methyl-morpholine; trifluoroacetic acid; isobutyl chloroformate; In dichloromethane;
DOI:10.1002/hlca.19910740505

Reference yield:

: 33014-68-5
tert-butoxycarbonyl-L-phenylalanyl-L-leucine

: 136860-12-3
N-(L-phenylalanyl-L-leucyl)-β-D-glucopyranosylamine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) isobutyl chloroformate, N-methylmorpholine / 1) THF, -15 deg C, 2 min, 2a) THF, H₂O, -15 deg C, 10 min, 2b) RT, overnight

2: 75 percent / CF₃CO₂H / CH₂Cl₂ / 0.5 h / Ambient temperature

With 4-methyl-morpholine; trifluoroacetic acid; isobutyl chloroformate; In dichloromethane;
DOI:10.1002/hlca.19910740505