Technology Process of C11H23NO2S
There total 5 articles about C11H23NO2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C15H31NO3S2;
With
hydrogenchloride; water;
In
tert-butyl methyl ether;
at 22 - 25 ℃;
for 1h;
pH=0.5 - 0.6;
Industry scale;
With
sodium hydroxide;
In
water;
at 22 - 30 ℃;
for 0.25h;
pH=>= 12;
Industry scale;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 4 h / 60 °C / Industry scale
2.1: n-butyllithium / hexane; tert-butyl methyl ether / 3.5 h / 0 - 3 °C / Industry scale
2.2: 1.5 h / 2 °C / Industry scale
3.1: hydrogenchloride; water / tert-butyl methyl ether / 1 h / 22 - 25 °C / pH 0.5 - 0.6 / Industry scale
3.2: 0.25 h / 22 - 30 °C / pH >= 12 / Industry scale
With
hydrogenchloride; titanium(IV) tetraethanolate; n-butyllithium; water;
In
tetrahydrofuran; hexane; tert-butyl methyl ether;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / hexane; tert-butyl methyl ether / 3.5 h / 0 - 3 °C / Industry scale
1.2: 1.5 h / 2 °C / Industry scale
2.1: hydrogenchloride; water / tert-butyl methyl ether / 1 h / 22 - 25 °C / pH 0.5 - 0.6 / Industry scale
2.2: 0.25 h / 22 - 30 °C / pH >= 12 / Industry scale
With
hydrogenchloride; n-butyllithium; water;
In
hexane; tert-butyl methyl ether;
