Trifluoro-acetic acid 1-ethoxy-2-[phenyl-(2,2,2-trifluoro-acetyl)-amino]-ethyl ester

Base Information

Chemical Name:Trifluoro-acetic acid 1-ethoxy-2-[phenyl-(2,2,2-trifluoro-acetyl)-amino]-ethyl ester
CAS No.:75948-78-6
Molecular Formula:C₁₄H₁₃F₆NO₄
Molecular Weight:373.252
Hs Code.:

Synonyms:Trifluoro-acetic acid 1-ethoxy-2-[phenyl-(2,2,2-trifluoro-acetyl)-amino]-ethyl ester

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Chemical Property of Trifluoro-acetic acid 1-ethoxy-2-[phenyl-(2,2,2-trifluoro-acetyl)-amino]-ethyl ester

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Technology Process of Trifluoro-acetic acid 1-ethoxy-2-[phenyl-(2,2,2-trifluoro-acetyl)-amino]-ethyl ester

There total 4 articles about Trifluoro-acetic acid 1-ethoxy-2-[phenyl-(2,2,2-trifluoro-acetyl)-amino]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75934-33-7
N-(2,2-Diethoxy-ethyl)-2,2,2-trifluoro-N-phenyl-acetamide

: 407-25-0
trifluoroacetic anhydride

: 383-63-1
ethyl trifluoroacetate,

: 75948-78-6
Trifluoro-acetic acid 1-ethoxy-2-[phenyl-(2,2,2-trifluoro-acetyl)-amino]-ethyl ester

Guidance literature:: for 0.0833333h; ice bath;
DOI:10.1021/jo00317a026

Reference yield:

: 22758-34-5
N-phenyl-2-aminoacetaldehyde diethylacetal

: 75948-78-6
Trifluoro-acetic acid 1-ethoxy-2-[phenyl-(2,2,2-trifluoro-acetyl)-amino]-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / triethylamine / hexane / ice-water bath, then room temperature, 1 h

2: 0.08 h / ice bath

With triethylamine; In hexane;
DOI:10.1021/jo00317a026

Reference yield:

: 62-53-3
aniline

: 75948-78-6
Trifluoro-acetic acid 1-ethoxy-2-[phenyl-(2,2,2-trifluoro-acetyl)-amino]-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / NaHCO₃ / aq. ethanol / 96 h / Heating

2: 97 percent / triethylamine / hexane / ice-water bath, then room temperature, 1 h

3: 0.08 h / ice bath

With sodium hydrogencarbonate; triethylamine; In ethanol; hexane;
DOI:10.1021/jo00317a026