(hydroxy(tosyloxy)iodo)pentafluorobenzene

Base Information

Chemical Name:(hydroxy(tosyloxy)iodo)pentafluorobenzene
CAS No.:111873-52-0
Molecular Formula:C₁₃H₈F₅IO₄S
Molecular Weight:482.167
Hs Code.:

Synonyms:(hydroxy(tosyloxy)iodo)pentafluorobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (hydroxy(tosyloxy)iodo)pentafluorobenzene

Chemical Property:

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Technology Process of (hydroxy(tosyloxy)iodo)pentafluorobenzene

There total 3 articles about (hydroxy(tosyloxy)iodo)pentafluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 14353-88-9
iodopentafluorobenzene bis(trifluoroacetate)

: 104-15-4
toluene-4-sulfonic acid

: 111873-52-0
(hydroxy(tosyloxy)iodo)pentafluorobenzene

Guidance literature:: In acetonitrile; at 0 - 25 ℃; for 2h; Inert atmosphere;

Reference yield: 87.0%

: 827-15-6
1,2,3,4,5-pentafluoro-6-iodobenzene

: 104-15-4
toluene-4-sulfonic acid

: 111873-52-0
(hydroxy(tosyloxy)iodo)pentafluorobenzene

Guidance literature:: 1,2,3,4,5-pentafluoro-6-iodobenzene; With oxone||potassium monopersulfate triple salt; trifluoroacetic acid; In chloroform; at 20 ℃; for 2h;

toluene-4-sulfonic acid; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1002/open.201402045

Reference yield:

: 827-15-6
1,2,3,4,5-pentafluoro-6-iodobenzene

: 111873-52-0
(hydroxy(tosyloxy)iodo)pentafluorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: Oxone / chloroform / 0 °C

2: acetonitrile / 2 h / 0 - 25 °C / Inert atmosphere

With Oxone; In chloroform; acetonitrile;