hexakis(2,4-tri-t-butyl-phenyl isocyanide)tungsten

Base Information

• Chemical Name: hexakis(2,4-tri-t-butyl-phenyl isocyanide)tungsten
• CAS No.: 98161-17-2
• Molecular Formula: C₁₁₄H₁₇₄N₆W
• Molecular Weight: 1812.53
• Mol file: 98161-17-2.mol

Synonyms:hexakis(2,4-tri-t-butyl-phenyl isocyanide)tungsten

Chemical Property of hexakis(2,4-tri-t-butyl-phenyl isocyanide)tungsten

Chemical Property:

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Technology Process of hexakis(2,4-tri-t-butyl-phenyl isocyanide)tungsten

There total 1 articles about hexakis(2,4-tri-t-butyl-phenyl isocyanide)tungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2,4,6‐tri‐tert‐butylphenylisocyanide (69847-28-5) + tungsten(VI) chloride (13283-01-7) → hexakis(2,4-tri-t-butyl-phenyl isocyanide)tungsten (98161-17-2)

Guidance literature:

With Na#Hg; In tetrahydrofuran; soln. of W compd. and isococyanide deriv. was added to Na amalgam (1,2%) and stirred for 3 h at room temp.; soln. was filtered, residue washed with THF, combined solns. were concd. and formed crystals dried under vac.; elem. anal.;

DOI:10.1016/0022-328X(85)87169-2

upstream raw materials:

2,4,6‐tri‐tert‐butylphenylisocyanide

tungsten(VI) chloride

Refernces