Technology Process of C35H51NO5Si
There total 4 articles about C35H51NO5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C37H55NO5Si;
With
Grubbs catalyst first generation;
In
dichloromethane;
at 50 ℃;
for 24h;
With
lead(IV) tetraacetate;
at 20 ℃;
optical yield given as %de;
DOI:10.1016/j.bmcl.2011.01.134
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C
2.1: Grubbs catalyst first generation / dichloromethane / 24 h / 50 °C
2.2: 20 °C
With
Grubbs catalyst first generation; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
DOI:10.1016/j.bmcl.2011.01.134
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium sulfate; triethylamine / dichloromethane / 3 h / 20 °C
2.1: sodium tetrahydroborate / ethanol / 1 h / 20 °C
3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C
4.1: Grubbs catalyst first generation / dichloromethane / 24 h / 50 °C
4.2: 20 °C
With
Grubbs catalyst first generation; dmap; sodium tetrahydroborate; magnesium sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.01.134