α-[(diisopropylamino)ethyl]-α-[(dimethylamino)ethyl]-p-tert-butylphenylacetamide

Base Information

Chemical Name:α-[(diisopropylamino)ethyl]-α-[(dimethylamino)ethyl]-p-tert-butylphenylacetamide
CAS No.:74792-31-7
Molecular Formula:C₂₄H₄₃N₃O
Molecular Weight:389.625
Hs Code.:

Synonyms:α-[(diisopropylamino)ethyl]-α-[(dimethylamino)ethyl]-p-tert-butylphenylacetamide

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Chemical Property of α-[(diisopropylamino)ethyl]-α-[(dimethylamino)ethyl]-p-tert-butylphenylacetamide

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Technology Process of α-[(diisopropylamino)ethyl]-α-[(dimethylamino)ethyl]-p-tert-butylphenylacetamide

There total 4 articles about α-[(diisopropylamino)ethyl]-α-[(dimethylamino)ethyl]-p-tert-butylphenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 74789-02-9
2-(4-tert-Butyl-phenyl)-4-diisopropylamino-2-(2-dimethylamino-ethyl)-butyronitrile

: 74792-31-7
α-[(diisopropylamino)ethyl]-α-[(dimethylamino)ethyl]-p-tert-butylphenylacetamide

Guidance literature:: With sulfuric acid; In acetic acid; for 24h; Heating;
DOI:10.1021/jm00184a008

Reference yield:

: 3288-99-1
4-tert-butylbenzyl cyanide

: 74792-31-7
α-[(diisopropylamino)ethyl]-α-[(dimethylamino)ethyl]-p-tert-butylphenylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / NaNH₂ / toluene / 0.5 h / 80 - 85 °C

2: NaNH₂ / 1.) toluene, 100 deg C, 10 min, 2.) toluene, reflux, 45 min

3: 51 percent / aq. H₂SO₄ / acetic acid / 24 h / Heating

With sulfuric acid; sodium amide; In acetic acid; toluene;
DOI:10.1021/jm00184a008

Reference yield:

: 74788-90-2
2-(4-tert-Butyl-phenyl)-4-diisopropylamino-butyronitrile

: 74792-31-7
α-[(diisopropylamino)ethyl]-α-[(dimethylamino)ethyl]-p-tert-butylphenylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: NaNH₂ / 1.) toluene, 100 deg C, 10 min, 2.) toluene, reflux, 45 min

2: 51 percent / aq. H₂SO₄ / acetic acid / 24 h / Heating

With sulfuric acid; sodium amide; In acetic acid;
DOI:10.1021/jm00184a008